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Analytical Data <br /> Client: SECOR International. Inc. Job Number: 720-7408-1 <br /> Client Sample ID: B-11 @ 50' <br /> Lab Sample ID: 720-7408-10 Date Sampled: 01/19/2007 1430 <br /> Client Matrix: Solid Date Received: 01/23/2007 0945 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 82608 Analysis Batch: 720-17644 Instrument ID: Varian 3900E <br /> Preparation: 5030B Prep Batch: 720-17645 Lab File ID: c:\varianws\data\200701\01 <br /> Dilution: 200 Initial Weight/Volume: 5.44 g <br /> Date Analyzed: 01/26/2007 1527 FinalWeighWolume: 10 mL <br /> Date Prepared: 01/26/2007 1553 <br /> Analyte DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 0.92 <br /> Benzene ND 0.92 <br /> Ethanol ND 230 <br /> Ethylbenzene ND 0.92 <br /> MTBE 8.0 0.92 <br /> TAME ND 0.92 <br /> Toluene ND 0.92 <br /> Xylenes, Total ND 1.8 <br /> TBA ND 1.8 <br /> DIPE ND 0.92 <br /> EDB ND 0.92 <br /> Gasoline Range Organics(GRO)-C6-C12 ND 46 <br /> Ethyl tert-butyl ether ND 0.92 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8(Surr) 109 50-130 <br /> 1,2-Dichloroethane-d4(Surr) 131 60- 140 <br /> STL San Francisco Page 15 of 63 <br />