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Analytical Data <br /> Client: SECOR International, Inc. Job Number: 720-7408-1 <br /> Client Sample ID: B-11 <br /> Lab Sample ID. 720-7408-12 Date Sampled: 01/19/2007 1440 <br /> Client Matrix: Water Date Received: 01/23/2007 0945 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch: 720-17632 Instrument ID: Saturn 3900B <br /> Preparation: 5030B Lab File ID: c:\saturnws\data\200701\01 <br /> Dilution: 200 Initial Weight/Volume: 40 mL <br /> Date Analyzed: 01/26/2007 1155 Final Weight/Volume: 40 mL <br /> Date Prepared: 01/26/2007 1155 <br /> Analyte Result(ug/L) Qualifier RL <br /> 1,2-Dichloroethane ND 100 <br /> Benzene ND 100 <br /> Ethanol ND 50000 <br /> Ethylbenzene ND 100 <br /> TAME 160 100 <br /> Toluene ND 100 <br /> Xylenes,Total ND 200 <br /> TBA 7700 1000 <br /> DIPE ND 200 <br /> EDB ND 100 <br /> Gasoline Range Organics(GRO)-C6-C12 ND 10000 <br /> Ethyl tert-butyl ether ND 100 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-l8(Sure) 99 77-121 <br /> 1,2-Dichloroethane-d4(Surr) 106 73- 130 <br /> STL San Francisco Page 18 of 63 <br />