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Analytical Data <br /> Client: SECOR International, Inc. Job Number: 720-7408-1 <br /> Client Sample ID: B-10 @ 35' <br /> Lab Sample ID: 720-7408-5 Date Sampled: 01/18/2007 1515 <br /> Client Matrix: Solid Date Received: 01/23/2007 0945 <br /> 8015B Nonhalogenated Organics using GC/FID-Modified(Diesel Range Organics) <br /> Method: 8015B Analysis Batch:720-17745 Instrument ID: HP DR05 <br /> Preparation: 3550B Prep Batch: 720-17537 Lab File ID: N/A <br /> Dilution: 1.0 Initial Weight/Volume: 30.30 g <br /> Date Analyzed: 01/24/2007 1902 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/24/2007 1348 Injection Volume: <br /> Column ID: PRIMARY <br /> Analyte DryM Corrected: N Result(mg/Kg) Qualifier RL <br /> Diesel Range Organics[C9-624] Np 0.99 <br /> Surrogate %Rec Acceptance Limits <br /> o-Terphenyl — — --- - <br /> 73 50- 130--- <br /> STL San Franri%rn Pac7e 24 of 63 <br />