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CHROMALAB, INC. V=nEnvironmental Services(SDB) October 14 , 1996 Submission #• 9610054 P G & E LAB Atten: David Harnish/John Holliday Protect MCDONALD ISLAND K3/K4 Project# 2774 MD Received: October 3, 1996 re: One sample for Volatile Organics by GC/MS analysis Method- SW846 METHOD 8240A, July 1992 Cl z en t Sample _TD: 1.2 Spl# 102682 Matrix: SOIL Sampled- October 2, 1996 Run# 3575 Analyzed October 12, 1996 REPORTING BLANK BLANK DILUTION RESULT LIMIT RESULT SPIKE FACTOR ANALYTE u K u K u K ACETONE 930 90 N.D -- 4 BENZENE N.D 22 N D 94 0 4 BROMODICHLOROMETHANE N D. 22 N D 4 BROMOFORM N D. 22 N D 4 BROMOMETHANE N D 22 N.D -- 4 METHYL ETHYL KETONE 180 90 N D -- 4 CARBON TETRACHLORIDE N.D 22 N D -- 4 CHLOROBENZENE N D 22 N D. 89 1 4 CHLOROETHANE N D 22 N.D - 4 CHLOROETHYLVINYLETHER N D 45 N D -- 4 HLOROFORM N D 22 N D -- 4 CHLOROMETHANE N.D 45 N D. -- 4 DIBROMOCHLOROMETHANE N D. 22 N.D. - - 4 1, 1-DICHLOROETHANE N D 22 N.D -- 4 1, 2--DICHLOROETHANE N.D 22 N D -- 4 1, 1-DICHLOROETHENE N D 22 N D. 92 7 4 1, 2-DICHLOROETHENE (CIS) N D 22 N.D -- 4 1, 2-DICHLOROET14ENE (TRANS) N D 22 N D -- 4 1, 2-DICHLOROPROPANE N.D 22 N D 4 CIS-1, 3-DICHLOROPROPENE N D 22 N D. 4 TRANS-I, 3-DICHLOROPROPENE N D 22 N.D. -- 4 ETHYLBENZENE 140 22 N D -- 4 2-HEXANONE N D 90 N D. -- 4 METHYLENE CHLORIDE N D 45 N D. -- 4 METHYL ISOBUTYL KETONE 170 90 N D -- 4 STYRENE N D 22 N.D 4 1, 1, 2, 2-TETRACHLOROETHANE N D 22 N D. -- 4 TETRACHLOROETHENE N.D 22 N D. - 4 TOLUENE 67 22 N.D 92 0 4 1, 1, 1-TRICHLOROETHANE N D 22 N D -- 4 1, 1, 2-TRICHLOROETHANE N D 22 N D. -- 4 TRICHLOROETHENE N.D 22 N.D. 95 2 4 TRICHLOROFLUOROMETHANE N D 22 N.D -- 4 VINYL ACETATE N D 220 N.D -- 4 ' VINYL CHLORIDE N D. 22 N D. 4 TOTAL XYLENES 740 22 N D 4 Note Reporting limits raised due to high Ievels of target & non-target compounds 1111-866-1681 ,, mw 1220 Quarry Lane • Pleasanton, California 94566-4756 (510) 484-1919• Facsimile (510) 484-1096 V05100C0405JiEWEF105T Federal 1D #68-0140157