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CH RQMALAB, INC. Environmental Services(SDB) October 14, 1996 Submission #. 9610054 P G & E LAB Atten: David Harni.sh/John Holliday Protect: MCDONALD ISLAND K3/K4 Project#: 2774 MD Received. October 3 , 1996 re One sample for Volatile Organics by GC/MS analysis Method SW84 6 METHOD 8240A, July 1992 Claent Sample ID. 10 Spl#: 102680 Matrix SOIL Sampled: October 2, 1996 Run# 3575 Analyzed October 11, 1996 REPORTING BLANK BLANK DILUTION RESULT LIMIT RESULT SPIKE FACTOR ANALYTE u K u K u K $ ACETONE N D 20 N D -- 1 BENZENE N D 5 0 N D 94 0 1 BROMODICHLOROMETHANE N D 5 0 N D `- 1 BROMOFORM N D 5 0 N D 1 BROMOMETHANE N D 5 0 N D -- 1 METHYL ETHYL KETONE N D 20 N D. -- 1 CARBON TETRACHLORIDE N.D 5 0 N D. -- 1 CHLOROBENZENE N.D. 5 0 N D 89 1 1 CHLOROETHANE N.D. 5 0 N D -- PH1 CHLOROETHYLVINYLETHER N D 10 N D -- 1 HLOROFORM N D 5 0 N D -- 1 CHLOROMETHANE N D 10 N D -- 1 DIBROMOCHLOROMETHANE N D 5 0 N D -- 1 1, 1-DICHLOROETHANE N D 5 0 N D -- 1 1, 2-DICHLOROETHANE N.D. 5 0 N D --- 1 1, 1-DICHLOROETHENE N D 5 0 N D 92 7 1 1, 2-DICHLOROETHENE (CIS) N D 5 0 N D -- 1 1, 2-DICHLOROETHENE (TRANS) N D 5 0 N.D -- 1 1, 2-DICHLOROPROPANE N D 5 0 N D. 1 CIS-1, 3-DICHLOROPROPENE N.D 5 0 N D 1 TRANS-I, 3-DICHLOROPROPENE N.D 5 0 N D -- 1 ETHYLBENZENE N.D 5 0 N D -- 1 2-HEXANONE N.D 20 N D -- 1 METHYLENE CHLORIDE N D 10 N.D -- 1 METHYL ISOBUTYL KETONE N D 20 N D -- 1 STYRENE N.D 5 0 N D -- 1 1, 1, 2 , 2-TETRACHLOROETHANE N.D 5 0 N D 1 TETRACHLOROETHENE N D 5 0 N D -- 1 TOLUENE N D 5 0 N D 92 0 1 1, 1 , 1-TRICHLOR0ETHANE N D 5 0 N.D -- 1 1, 1, 2-TRICHLOROETHANE N D 5 0 N.D -- 1 TRICHLOROETHENE N D 5 0 N D. 95 .2 1 TRICHLOROFLUOROMETHANE N D 5 0 N D -- 1 VINYL ACETATE N.D 50 N D -- 1 1 VINYL CHLORIDE N D 5 0 N D __ 1 TOTAL XYLENES N D 5 0 N.D 1 ne Zhao C ip Poali.nelli FU i emist Operations Manager 1110-1161-16111 G1 10110 1220 Quarry Lane•Pleasanton, California 94566-4756 (510)484-1919 • Facsimile (510) 484-1096 V651 O0004�SJIEWEI105] Federal ID #68-0140157