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Sequoia 680 Chesapeake Dnve Redwood City,CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Vget Cane Walnut Creek,CA 94598 (510) 988 9600 FAX 510)988 9673 <br /> ,!DAnalytical 899 Striker Avenue Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> 0b5 Services Client Project ID Tosco #0187, 437 E Miner Ave , Stockton <br /> 2401 Stanwell Dr, Ste 300 Matrix Liquid <br /> Concord, CA 94520 <br /> Attention Jarrell Crider QC Sample Group 7050162-169 Reported May 13, 1997 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Benzene Toluene Ethyl Xylenes <br /> Benzene <br /> Method EPA 8020 EPA 8020 EPA 8020 EPA 8020 <br /> Analyst K Nill K Nill K Nill K Nill <br /> MS/MSD <br /> Batch# 7050069 7050069 7050069 7050069 <br /> Date Prepared 5/5/97 5/5/97 5/5/97 5/5/97 <br /> Date Analyzed 5/5/97 5/5/97 5/5/97 5/5/97 <br /> Instrument I D # HP-4 HP-4 HP-4 HP-4 <br /> Conc Spiked 20yg/L 20ug/L 20pg/L 60pg/L <br /> Matrix Spike <br /> % Recovery 75 80 80 83 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery 85 90 85 83 <br /> Relative% <br /> Difference 13 12 6 1 00 <br /> LCS Batch# 4LCS050597 4LCS050597 4LCS050597 4LCS050597 <br /> Date Prepared 5/5/97 5/5/97 5/5/97 5/5/97 <br /> Date Analyzed 5/5/97 5/5/97 5/5/97 5/5/97 <br /> Instrument I D # HP-4 HP-4 HP-4 HP-4 <br /> LCS % <br /> Recovery 80 85 80 85 <br /> % Recovery <br /> Control Limits 60 140 60-140 60-140 60-140 <br /> Please Note <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> i <br /> SEQUOIA ANALYTICAL, #1271 preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> leature on File the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LGS recovery is to be used to validate the batch <br /> Alan B Kemp <br /> Project Manager <br /> 7050162 MPD X57 <br />