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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> E4 McCalnpbell Analytical Inc Telephone 925-798 1620 Fax 925-798-1622 <br /> http JJwww mccampbell.corn E-mail matn@mccampbell corn <br /> Env Science Associates Client Project ID #200252,UOP-MTBE Date Sampled 08/21/02 <br /> 225 Bush Street, Ste 1700 Date Received 08/21/02 <br /> San Francisco, CA 94104 Client Contact Peter HudsonDate Extracted 08122/02-08123102 <br /> Client P O Date Analyzed 08/22/02-08/23102 <br /> Oxygenated Volatile Organics by P&T and GC/MS* <br /> EaututionMethod SW50311B Analytical Method SW8260B Work Ordcr 0209372 <br /> Lab ID 0208372-OOIB 0208372-002B 1 0208372-0038 0208372-004B <br /> Client ID MW-1 MW-2 MW-3 MW-4 Reporting Limit for <br /> Matrix W � W W W <br /> DF=1 <br /> DF 1 1 ! 1 S W <br /> Compound Concentration ug/kg µg/L <br /> Dusopropyl ether(RIPE) ND ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND ND NO NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 5 0 <br /> Methanol ND ND<600 ND ND NA 500 <br /> Ethanol ND ND ND ND NA 50 <br /> !,2-Dtbromoethane(EDS) ND ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 994 889 989 986 <br /> Cdtnments <br /> *water and vapor samples and all TCL?&SPLP extracts are reported to ug/L,soil/sludge/sohd samples in ug/kg, wipe samples to ug/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> -- - -_ -- =organic content — _ — - _ --- - _ --- -- — -- _ -— _----_- --— - -- <br /> DHS Certificaton No 1644 Edward Hamilton,Lab Director <br />