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' 110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCalnpbell Analytical Inc Telephone 925 798 1620 Pax 925-798-1622 <br /> ' http//www mccampbell com E mail mmin@mccampbell com <br /> . Advanced GeoEnvirorunental, Inc Client Project ID Shockey&Sons Date Sampled 09/17/02 <br /> ' 837 Shaw Road Date Received 09/18/02 <br /> Stockton, CA 95215 Client Contact Bill Little Date Extracted 09/21/02-09/24/02 <br /> Client P O Date Analyzed 09121102-09124/02 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0209270 <br /> ' Lab ID 0209270-001B � 0209270-002B 10209270-003B <br /> Client ID MW1/09-17-02 { MW2/09-17-02 j MW3/09-17-02 <br /> Reporting Limit for <br /> ' Matrix W W W DF=1 <br /> DF 1 � 1 1 S w <br /> ' Compound Concentration uglkg µg1[, <br /> tert-Amyl methyl ether(1 AME) ND ND ND NA 05 <br /> ' Benzene ND ND ND NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND NA 5 0 <br /> Dusopropyl ether(DIPS) ND ND ND NA 0 5 <br /> Ethylbenzene ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND NA 0 5 <br /> ' Methyl-t-butyl ether(MTBE) ND ND ND NA 0 5 <br /> Toluene 0 55 ND ND NA 0 5 <br /> Xylenes ND ND ND NA 0 5 <br /> ' Surrogate Recoveries(%) <br /> %SS 98 9 995 998 <br /> ' Comments h <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludgc/solld samples in ug(kg, wipe samples to ug/wipe, <br /> productioil/non-aqueous liquid samples in mglL <br /> ND means not detected above the reporting hint,NIA means analyte not applicable to this analysts <br /> ' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,a)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br />