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McCAMPBELL ANALYTICAL INC. 110 2nd Avenue South,#D7,Pacheco,CA 94553 <br /> Tele:510-798-1620 Fax: 510-798-1622 <br /> i <br /> Advanced GeoEnvironmental Client Project ID: Shockey Trucking Date Sampled: 06106-06107196 <br /> 1803 West March Lane,Ste. A Date Received:06/08/96 <br /> Stockton, CA 95207 Client Contact: Bill Little Date Extracted:06/10/96 <br /> Client P.O: Date Analyzed:06/10/96 <br /> Gasoline Range(C6-Cl2) Volatile Hydrocarbons as Gasoline*,with MTBE&BTEX* <br /> EPA methods 5030.modified 8015.and 8020 or 602;California RW C8 SF Ha Region method GCFID(5030 <br /> Lab ID Client ID Matrix TPH(g)+ MTBE Benzene Toluene Ethylben- Xylenes % Rec. <br /> zene Surrogate <br /> 65765 B1-19' S 32,g ND ND ND ND 0.015 97 <br /> 65766 B2-20' S ND ND ND ND ND ND 102 <br /> 65767 B3-20' S ND ND ND ND ND ND 103 <br /> 65768 B4-10' S 120,g ND< 0.04 ND 0.02 0.04 0.26 95 <br /> 65769 B4-15' S 720,g ND< 0.2 ND< 0.05 0.12 0.59 1.6 98 <br /> 65770 B4-19' S 620„ ND< 0.2 ND< 0.05 0.10 0.26 1.3 102 <br /> • <br /> Reporting Limit unless W 50 ug/L 5.0 0.5 0.5 0.5 0.5 <br /> otherwise stated;ND <br /> means not detected <br /> above the reporting limit S 1.0 mg/kg 0.05 0.005 0.005 0.005 0.005 <br /> * water and vapor samples are reported in ug/L,soil samples in mg/kg,and all TCLP extracts in mg/L <br /> # cluttered chromatogram;sample peak coelutes with surrogate peak <br /> + The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not <br /> responsible for their interpretation: a) unmodified or weakly modified gasoline is significant;b)heavier gasoline <br /> range compounds are signsficant(agedgosoline?);c}lighter gasoline range compounds(the most mobile fraction) <br /> are significant; d) �asoTlme range compounds having broacfchromatographic peaks are significant; biologically <br /> altered gasoline?; e) TPH pattern that does not appear to be derived from gasoline (?); 0 one to a few isolated <br /> peaks present;g)stronglyaged asoline or diesel range compounds are significant;h)lighter than water immiscible <br /> 0 sheen is present;i) liquid sample that contains greater than— 5 vol.% sediment;j}no recognizable pattern. <br /> DH S Certification No. 1644 Edward Hamilton,Lab Director <br />