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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 9455 3-5 560 <br /> McCA1MPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ZO http//www mccampbell coin E-mail main@mccampbell com <br /> ' Advanced GeoEnvironmental Client Project ID Chet's Auto Date Sampled 10/23-24/01 <br /> 837 Shaw Road Date Received 10/25/01 <br /> Stockton, CA 95215 Client Contact Bill Little Date Extracted 10/31/01 <br /> ' Client P O I Date Analyzed 10/31/01 <br /> Volatile Orgames By GCIMS <br /> EPA method 8260 <br /> ' Lab ID 82012 <br /> Cilent ID B1-Hz0 65 <br /> Matrix W <br /> Compound Concentration* R�s <br /> Compound Concentration* Rep=ng Llmkl <br /> 1 W S <br /> Acetone ib) ND<10 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 -)0 <br /> ' Bromoberizene ND 10 50 Ethylbenzene 11 10 )0 <br /> Bromochloromethane NO 1 0 50 1lexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 5 0 lodomethane ND 1 0 5 0 <br /> Bromoform ND 10 50 lsopropylbenzene 12 10 5 0 <br /> ' Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene 18 l 0 5 0 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 10 5 0 Methylene Chlunde` ND<2 0 10 50 <br /> ten-Butyl benzene ND 10 5 0 Methyl ethyl ketone t ND 2 0 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone ND 10 5 0 <br /> Carbon retrachlonde ND 10 50 Methyl tent-Butyl Ether(MTBE) 10 50 <br /> Chlorobenzene ND l 0 5 0 Naphthalene 91 50 5 0 <br /> Chloroethane ND 1 0 5 0 n-Propyl benzene 4 l 10 5 0 <br /> 2-Chloraethyl Vinyl Ethe ND 10 5 0 Styrene ND 10 5 0 <br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 l,l 2 2-Tetrachloroethane ND I O 50 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND 10 5 0 <br /> ' 4-Chlorotoluene ND l 0 50 Toluene 91 10 50 <br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1 2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND to 5 0 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> ' 1,2-Dichlorobenzene ND l0 50 1,1,2-Tnchloroethane ND 10 50 <br /> 1 3-Dichlorobenzene ND 10 50 Tnchlornethene ND 10 50 <br /> 1,4-Dichlorobenzene ND l 0 5 0 Tnchlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 1 0 5 0 <br /> ' 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene 23 1 0 50 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene 2 9 10 5 0 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate '° ND 50 25 <br /> cis-l,2-Dichloroethene ND 1 0 50 Vinyl Chloride " ND 10 50 <br /> trans-l,2-Dichloroethene ND 1 0 5 0 Xylenes,total 66 10 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries{%) <br /> 2 2-Dichloropropane ND 10 5 0 Dtbromofluoromethane 106 <br /> ' <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 102 <br /> cis-1,3-Dichloropropene ND 1 0 5 0 4-Bromoiluorobenzene 98 <br /> water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chlomethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopmpylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than—5 vol % <br /> sediment, {1) sample diluted due to high organic content, (k) ethenylbenzene (1 methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hanulton,Lab Director <br /> I <br />