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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209) 572-0916 <br /> �eport# M35I-13 <br /> CERTIFICATE OF ANALYSIS Date: 12/28/01 <br /> Date Rec'd: 12/17/01 <br /> HF Environmental Date Started: 12/20/01 <br /> PO Box 427 Project: Eckert Cold Storage Quarterly Date Completed: 12/27/01 <br /> Oakdale CA 95361 <br /> Date Sampled: 12/17/01 <br /> PO# Time: 12:22pm <br /> Sample ID: MW 1 Sampler : R Azevedo(Geo) <br /> Lab ID: M312466 <br /> ' Method RL Analyte Results Units <br /> 8260B 6.0 Benzene 270 pg/L <br /> 6.0 Toluene ND <br /> ' 6.0 Ethyl Benzene 115 <br /> 12 Total Xylenes 42 <br /> 20 Methyl tert-butyl ether (MTBE) ND <br /> ' 800 Ethanol ND <br /> 400 tert-Butanol ND <br /> 20 di-Isopropyl ether •(DIPE) ND <br /> 20 Ethyl Cert-butyl ether (ETBE) ND <br /> 20 tert-Amyl methyl ether (TAME) ND <br /> 20 Ethylene dibromide (ED13) ND <br /> 10 1,2-Dichloroethane (1,2-DCA) ND <br /> Surrogate A=t Spiked Amnt Recovered %Recovery OC Limit% <br /> ' 1,2-Dichloroethane-d, 100 108 108.0 72-132 <br /> 2-Bromo-l-chloropropane 100 113 113.0 71-134 <br /> 4-Bromofluorobenzene 100 83.1 83.1 74-132 <br /> X <br /> ' ario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />