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GeoAnaiY tical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209) 572-0916 <br /> eport# M351-13 CERTIFICATE OF ANALYSIS Date: 12/28/01 <br /> Date Recd: 12/17/01 <br /> (HF Environmental Date Started: 12/20/01 <br /> PO Box 427 Project: Eckert Cold Storage Quarterly Date Completed: 12/27/01 <br /> Oakdale CA 95361 Date Sampled: 12/17/01 <br /> PO# Time: 6:30am <br /> Sample ID: Trip Blank Sampler : R Azevedo(Geo) <br /> Lab ID: M312474 <br /> Method RL Analyte Results Units <br /> 8260B 0.3 Benzene ND p /L <br /> 0.3 Toluene ND <br /> 0.3 Ethyl Benzene ND <br /> 0.6 Total Xylenes ND <br /> 1.0 Methyl tert-butyl ether (MTBE) ND <br /> t 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1.0 di-Isopropyl ether'(D1PE) ND <br /> 1.0 Ethyl tert-butyl ether (ETBE) ND <br /> 1.0 tert-Amyl methyl ether (TAME) ND <br /> 1.0 Ethylene dibromide (EDB) ND <br /> 0.5 1,2-Dichloroethane (1,2-DCA) ND <br /> 1 <br /> 1 <br /> 1 <br /> Surrogate Amnt Spiked A=t Recovered %Recovery QC Limit% <br /> ' 1,2-Dichloroethane-d4 5.00 6.79 135.8 72-132 <br /> W 2-Bromo-l-chloropropane 5.00 5.07 101.4 71-134 <br /> 4-Bromofluorobenzene 5.00 4.62 92.4 74-132 <br /> 1 <br /> ' Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />