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1 GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> eeport# M253,11 CERTIFICATE OF ANALYSIS Date: 4/14/01 <br />' Date Rec'd: 9/10/01 <br /> WHF Environmental Project: Eckert Cold Storage - Quarterly Date Started: 9/12/01 <br /> PO Box 427 Date Completed: 9/14/01 <br /> Oakdale CA 95361 PQ# Date Sampled: 9/10/01 <br /> Time: <br /> Sample ID: MW-8 Sampler : R Azevedo(Geo)/R <br />'Lab ID: M308855 <br /> Method RL Analyte, Results Units <br /> 8260B 24 Benzene 2000 pg/L <br /> 1.2 Toluene 33 <br /> 24 Ethyl Benzene 1800 <br /> 48 Total Xylenes 1800 <br /> 4.0 Methyl tert-butyl ether (MTBE) 34 <br /> 160 Ethanol ND <br /> 80 tert-Butanol ND <br /> ' 4.0 di-Isopropyl ether (DIPE) ND <br /> 4.0 Ethyl tert-butyl ether (ETBE) ND <br /> 4.0 Cert-Amyl methyl ether (TAME) ND <br /> ' 4.0 Ethylene dibromide (EDB) ND <br /> 2.0 1,2-Dichloroethane (1,2-DCA) ND <br /> r <br /> ' Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 400 401 100.3 72-132 <br /> ' 2-Bromo-l-chloropropane 400 347 86.8 71-134 <br /> 4-Brorripfluorobenzene 400 430 107.5 74-132 <br /> Cw � � � <br /> Mario D'Onofr' Donna Zer <br /> ' Chemist Certification # 1157 Laboratory Director <br />