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110 2nd Avenue South,OD7,Pacheco.CA 94553-5560 <br /> 4 McCampbell Analytical, Inc. 'Felephene:925-798-162D Fax:925-798-1622 <br /> Website:www.mec"beil.coni E-mail:main ccmccampbell,com <br /> _ Advanced GeoEnvirontnental,Inc. Client Project ID: Local Food Store Date Sampled: 05/26/04 <br /> 837 Shaw Road Date Received: 05/27/04 <br /> Client Contact: Paul Dotson Date Extracted: 05127104-05128104 <br /> Stockton, CA 95215 <br /> Client P.O.: I Date Analyzed: 05127104-05128/04 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Fxtr-action Method: SW503DB Analytical Method:SW8260B Work Order:0405430 <br /> Lab ID 0405430-OOIB 0405430-002B 0405430-003B 0405430-004B <br /> Client ID MW1 MW2 MW3 MW4 <br /> Reporting Limit for <br /> Matrix W W W W DF-1 <br /> 7FL l - - - 20 I 5 g W <br /> Compound Concentration uQ'kg µ97 <br /> tert-Amyl methyl ether(TAME) ND ND<10 ND ND<2.5 NA 0.5 <br /> t-Butyl alcohol(TBA) ND ND<100 ND 31 NA 5.0 <br /> 1,2-Dibromoethane(EDB) ND ND<10 ND ND<2.5 NA 0.5 <br /> 12-Uichloroethane(1,2-DCA) NUND<IQ ND ND<2.5 NA Q.5 <br /> Diisopropyl ether(RIPE) ND ND<10 ND ND<2.5 NA 0.5 <br /> Ethyl tert-butyl ether(I-BE) ND ND<10 ND ND<2.5 NA 0.5 <br /> i <br /> Methyl-t-butyl ether(M"IBE) 2.3 210 ND 120 NA 0.5 <br /> Surrogate Recoveries(%) <br /> °/0SS: 83.4 90.7 84.4 98.3 <br /> Comments i <br /> water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludgelsolid samples inµglkg, wipe samples in pg/wipe, <br /> prod uctioiI/non-aquems liquid samples in mg/L. <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis. <br /> 4 surrogate di luted out of range or surrogate coelutes with another peak. <br /> -- h)lighter than water immiscible sheen/product is present;i}liquid sample that contains greater than--1 vol.%sediment;j)sample diluted due to high <br /> organic content- <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />