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Jl <br /> 110 2nd Avenue South #D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925 798-1620 Fax 925-798 ifi22 <br /> httpJlwww meta bell tom E mail ma mccampbell tom <br /> Advanced GeoEnvironmental,Inc Client Project TD Local Food Store Date Sampled 09/18/03 <br /> 837 Shaw Road Date Received 09/19/03 <br /> Client Contact Paul Dotson Date Extracted 09/24/03-09125/03 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 09/24/03-09/25/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0309359 <br /> Lab ID 0309359-OOIC 0309359-002C 0309359-003C 0309359-004C <br /> Client ID M W I MW2 MW3 MW4 <br /> Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF 1 -- - 5 --- 5 200 S w <br /> Compound Concentration ug/kg Vg/L <br /> Dusopropyl ether(DIPS) ND ND<2 5 ND<2 5 ND<100 NA 05 <br /> Ethyl tert-butyl ether(ETRE) ND ND<2 5 ND<2 5 ND<100 NA 05 <br /> Methyl-t-butyl ether(MTBE) 96 160 160 3900 NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND<2 5 ND<2 5 ND<100 NA 05 <br /> t-Butyl alcohol(TBA) ND ND<25 ND<25 ND<1000 NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND<2 5 ND<2 5 ND<100 NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND<2 5 ND<2 5 ND<100 NA 05 <br /> Surrogate Recoveries(%} <br /> %SS 109 110 111 106 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soiUsludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 _Angela Rydelius,Lab Manager <br />