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1 <br /> I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ht //www mecam bell corn E-mail main@mccampbell cont <br />' Advanced GeoEnvironmental Client Protect ID MBP-Mossdale Date Sampled 09/27-09/28/00 <br /> 4005 North Wilson Way Date Received 10/03/00 <br />' Stockton, CA 95205 Client Contact Bill Little Date Extracted 10/03/00 <br />' Client P O Date Analyzed 10/08-10/10/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab[D 49312 <br /> Client ID MW3-15 <br /> Matrix S <br /> Compound Concentration* rias Si Compound Concentration* Rcpwuag L.Si <br />' Acetone(b) ND 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene ND 10 5 0 Ethylene dibromide ND to 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br />' Bromochloromethane ND 10 50 Hexachlorobutadiene ND 5 0 25 <br /> Bromedichloromethane ND 10 1 5 0 lodomethane ND 10 50 <br /> Bromoform ND to 5 0 Isopropylbcnzene ND 10 50 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 10 50 <br />' n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride() ND<10 10 50 <br /> teri-Butyl benzene ND 10 50 Methyl ethyl ketone ND 2 0 10 <br />' Carbon Disulfide ND 10 50 Methyl isobutyl ketone ND 10 50 <br /> Carbon Tetrachloride ND to 50 Methyl tert-Butyl Ether(MTBE) 10 5 0 <br /> Clilorobenzene ND 10 50 Naphthalene ND 50 50 <br /> Chloroethane ND 10 50 n-Propyl benzene ND to 50 <br /> 2-Chloroethyl Vinyl Eth ND 10 50 Styrene ND 10 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND l0 50 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND 10 5 0 <br /> 4-Chlorotoluene I ND 10 5 0 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnebloroethane ND 10 50 <br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Tnchloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 10 5 0 <br /> Dtchlorodifluoromethane ND 10 5 0 1,2,3-Tnchtoropropane ND 10 5 0 <br /> I 1,1-Dichloroethane ND 10 50 1,2,4-Trimethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> I,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate '° EEND <br /> 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chlonde ° 10 50 <br /> I trans-1,2-Dichloroethene ND l 0 50 Xylenes,total ND 10 50 <br /> 1,2-Dichloropmpane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND 10 50 i Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 78 <br /> 1,1-Dichloropropene ND 10 1 50 Toluene-d8 116 <br /> cis-1,3-Dichloropropene JL ND1 0 1 50 1 4-Bromofluorobenzene �E�J 139 <br /> 'water and vapor samples are reported in uglf,,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> . pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> I chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />