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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: ENSR Consulting dt Engmxrtng Service Request: 59701286 <br /> Project: Norcal/Stockton Scavenger CoJ9647-1.401 Date Collected: 6/30/97 <br />' Sample Matrix: Water Date Received: 7/3197 <br /> T'PH as Diesel <br />' Prep Method EPA 3510 Units uA(ppb) <br /> Analysis Method CA/LUFT Basis NA <br />' Test Notes <br /> Dilution Date Date Result <br /> Sample Name Lab Code MRL Factor Extracted Analyzed Result Notes <br /> MW-1 S9701286-001 50 1 7/8197 7/8197 ND DI <br /> MW-3 59701286-002 50 1 7/8/97 7/8/97 ND D2 <br />' MWA 59701286-003 50 1 7/8/97 7/8/97 ND D3 <br /> Method Blank 5970708 MB 50 1 7/8/97 7/8/97 ND <br /> 1 <br /> D1 Sample contained heavy oil at 98 ppb <br />' D2 Sample contained heavy oil at 140 ppb <br /> D3 Sample contained heavy oil at 170 ppb <br /> 1 1A=59-lp <br /> Page 3 <br />