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' COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: ENSR Consulting&Engmeenng Service Request: S9701416 <br /> Project- NorcaVStockton Scavenger/5027-002 Date Collected- 7116197 <br />' Sample Matrix Solid Date Received- 7/22197 <br /> BTEX and TPH as Gasoline <br /> rSample Name SVGAGI Umts mg/Kg(ppm) <br /> Lab Code S9701416-002 Basis Wet <br /> Test Notes <br /> Prep Analysts Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LUFT 1 20 7/29/97 7/30/97 840 <br />' Benzene EPA 5030 8020 0 005 20 7/29/97 7/30/97 1 1 <br /> Toluene EPA 5030 8020 0 005 20 7/29/97 7/30/97 88 <br /> Ethylbenzene EPA 5030 8020 0 005 20 7/29/97 7/30/97 64 <br /> Xylenes,Total EPA 5030 8020 0 005 20 7129/97 7130/97 24 <br /> nS22=0597p <br />' Page 3 <br />