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CD <br /> W <br /> HWM©a 1�MI CERTIFICATE OFANALYSIS <br /> Analytical LaboratCory N <br /> Tuestirt}),5farch 12,2002 t9 <br /> CD <br /> TO: Wi/liam Liifle <br /> Advanced GeoEnvironmental <br /> 837 Shaw Road <br /> Stockton CA 95215 1D <br /> Oxygenated Compound by GCMS <br /> N <br /> M <br /> Santpt a Information LD <br /> A <br /> Sample ID: 14494-04A Sample Type: Grab <br /> Sample Description: Tank#2 South EndProject Name: 4040 E.Main ST. <br /> Date/time Sampled: 3/6/2002 3:25;00 PM Sample Matrix: Soil m <br /> ANALYTICAL IlESUL.T QAIQC REPORT <br /> .__„�, .e.,.�,�...,...,, - --......n...�..,�..�..,..._.�.._»....,�.�...-.,..�..4.,...--.�b:� Date LCS Spike MS Spike �,.....,.�.F�.�........,.._,f.. . <br /> :Test Parameter Methal DLR Unit Result Analyzed Blank Conc. LCS% Cone. MN% MSD RSD <br /> Methyl t-Butyl Ether�MtBE) EPA 82508 5 ug/kg N D 08 tv1ar-02 ISD 12.6 112.5% 12.8 117.2°Yo 117.2% 0.0% <br /> iii-isopropyl ether(DIPE) EPA B280B 5 ugrkg ND 08-Mar-02 ND 35 98.5% 35 a2.9% 82.9% 0.0% <br /> Ethyl-t-butyl ether(ELBE) EPA 82606 5 ug4cg N D 08-Mar-02 ND 35 98.3% 35 108.6% 108.60/a 0.0% D <br /> Teri-amyl it sthyl ether(MIME) EPA 82fi0B 5 ug4cg NO 08War-02 ND 35 95.7% 35 100.2% 103.3%- 0.8% m <br /> t-Butanol(TBA) EPA B2t 0B 100 ug/kg NO 08-Mar-02 ND 100 110.0% 1:00 88.0% 86.05'o 0.6% o <br /> 1,2•Dlchloroerthane-d4(Surrogate) %Recovery 105°/ <br /> 4-B FB{Surrogate) %Recovery 104% Z <br /> mg(L=ntilligrorns per Liter—pptn RSD-rep.1mem relative perce+u dl&—ent(RPI)}between drtplicotes spike of samples <br /> uglL=mirrogrorns per Liter=ppb or DZT1k.-ate ojSmnple <br /> R FU B TTED, AMUSD-measure asure ojlke perrent recovery effirieucies within etre nvar•ix <br /> C=Conquosite G=Grab f.S <br /> L '-measure recovery percent reeorof dee Lrrbnruto+y Control Spike(L(.'S) <br /> V <br /> DLR-Detection Liadi for the Pugjose of Reporting. Exceptional sample. <br /> Ju i ath an Man T.Le,Laboratory Director marines or,inlet ferereaces may msuA in higher detection iineits <br /> -o <br /> D <br /> G) <br /> M <br /> M <br /> F.PA-Fa+irnnn:entat Protaction AgeirryAlelhod. Sbl.Staralrnrl d?etharl for Rrmniaotion ajlfrnter 1YaY+eivrtttr 13th EA. Page 1 of I <br /> 545 E. Cleveland St. Suite A Stockton. CA 95204 Tel.: !2091 462-0892 Fax: (209) 462-7935 <br />