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CD <br /> CERT'IF1 CAT'E OF ANALYSIS <br /> Araa/yttica/ Laboratory Tuesday,A1arch 12,2/1112 N <br /> TO: William Liftle m <br /> Advanced GocEnvironmenta! w <br /> 837 Shaw Road ` <br /> Stockton CA 95215 <br /> LD <br /> Oxygenated Compound by GCMS <br /> Sample Information <br /> LO <br /> Sample ID, 14494-01A Sample Type: Grab m <br /> Sample Description: sank#1 North End Project Name: 4040 E.Main,ST. <br /> DatelTime sampled: 3/612002 4:30:00 PM Sample Matrrx: Soil o <br /> ANALYTICAL RESULT QAIQCREPORT <br /> Date LCSSpike MS Spike .�:,,,.,,...,.,..<..d...�,t,.......a..,,.�.�.-. <br /> Test Parameter Method DLR Unlit Result Analyzed Blank Came. LCS% Cone. MS% MSD RSD <br /> Methyl t-Butyl Ether(MTBE) EPAMDB 5 ug/kg ND 08-Mar-D2 NO 12.8 112.5% 12.8 117.2% 117.2% 0.0% <br /> DI-isapro*other(DIPE) EPA826DB 5 uglkg NO 08-Mar-02 ND 35 98.5% 35 82.9% 82.9% 0.0% <br /> Ethyl-t-butyl other(ETBE) EPA 82608 5 uglkg ND 08•Mar--D2- ND 35 98.3% 35 108.6% 108.6% 0.0% <br /> (T y uglkg ND 08-Mar-02 ND 35.... ._ ..95.7% 35 100.2% 103.3% 0.8% m <br /> Tertamyl methyl ether AME EPA 82608 5 <br /> (TBA) gikg ND 08-Mar-02 ND 100 110.0% 100 88.4% 86.0% 0.6% U) <br /> -t�Btrtanfll TBA EPA 100 u <br /> 1,2 Dichloroethaned4(Surrogate} 96Recovery 110% <br /> 443FB{Surrogate) %Recovery 112% <br /> z <br /> 0 <br /> nig.!L=rniNtgrrrrrrs per tiler=pinn (RPD}befxcea dupIfealea•spike gl'sunmples <br /> ug:'L=urirroyratns per Liter=ppb <br /> W.Duplicate of Sample <br /> RESPE P'UL B 1TED, M&WISD-owasureofrhepememrecorerpeffiriewrieswith indrenvnrb: <br /> C=C'omporife C.=Grab <br /> LCS•-measure of ihr perre)tt rvrot,ert-of tlae L aborafwy Coalrol Spike a cs) <br /> J riat arc Hao 1.Le, Laboratory Director <br /> D1:R-DrurtionUaltforthePevposeol'Reponing- &a-preonrrisample- <br /> nraireres or inlet(errrreces•mrr}••rc:rult in Licher detection/emits <br /> D <br /> G) <br /> Fr] <br /> - m <br /> W <br /> tP t-Ea�iroionenral ProtecriorJ.fgerrcy A3etRort Sri4-Standar d dlethal ja Eznrnerrntion of l{'rater ff'astrvk-•rrter 1414 Ed. <br /> Page 1 of 1 <br /> 545 E. Cleveland St. Suite A Stockton, CA 95204 Tel.: (209) 462-0892 Fax: (209) 462-7955 <br />