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w <br /> CER TIFICA TE OF ANALYSIS <br /> .4.�aryti�ar iabor�z�ry <br /> Tuesday,Afarclr l2, 2002 ry <br /> TO: . William Little m <br /> m <br /> Advanced GeoEnvironmental w <br /> 837 Shaw Road <br /> Stockton CA 95215 <br /> Oxygenated COmPOLInd by GCVIS LD <br /> Sample Ifyin-trarion m <br /> Lo <br /> Sample ID: 1449342.A Sample Type: Composite p <br /> Cn <br /> Sample Description: SP3+SP4 Composite <br /> Project Name: 4040 E. Main ST. <br /> DaleMyne Sampled: 3/6/2002 1:45;00 PM Sample Matrix: Sail <br /> 00 <br /> ANALYTICAL RESULT QAIQCREPORT <br /> Date LCS Spike MS Spike <br /> :Test Parameler Method DLR Unit Result '?Analyzed Blank Cone. LCS% Cone_ MS% MSD RSD <br /> Methyl t-Butyn Ether(MtBE) EPA 82806 5 ug/kg NO 08-Mar-02 ND 12.8 112.5% 12.8 117.2% 117.2% 0.0% <br /> D1-lsopropyl ether(DIPS) EPA-8-2,6-09 5 u .. .__.-. .-_.. ....... ... .. ..._ _. . _.. . . . . <br /> g�9 NO 08-Mar-02 ND 33 98.596 355 82.9962.9% 82.996Eth0.05'0 <br /> yf utyl other(ETBE) EPA 8260B 5 ug/kg ND 08-Mar-02• ND 35 98.3% 35 108.6% 108.696 0.k <br /> Tert-amyl methyl ether(T/4Mk� EPA 82506 5 ug/kg NO 08-mar-02 ND 35 95.796 35 100.2% 403.3%% 0.896 m <br /> t-Butanol(TBty EPA 82608 :.. .......:.. ...., ..:. .-., .,...- _.... ..:._.. . --,. -.:, .. ,.,..,__ .. .... .-..... . . . ..... <br /> 700 ug/kg ND.. 0&Mar-02 ND s 100 f 10.0% 100 88.0% 85.0% 0.6% cn <br /> 1,20chloroethane-d4(Surrogate) %Recovery.....,..._.... _, ._ ,< ..a. , .0°rG ..x .-..... , ,. _. ._:.... . . _. o <br /> _. ...... <br /> 443PBgSurrog %Reco <br /> ' Ate} srgTy S"ru ..- .. . .._ . .. ... ... .._ � <br /> O <br /> milligrarrrs per Litre--ppn RSL)-neprr^senj rrlatiir prrcc�nr riifferext fRPO)be trseerr drrpficates•spike r�rsrunples <br /> ugIL=twit rogt tuns per Liter=pub or.Duplicate of salhple <br /> �' Z 'UL B 77ED, df:S rh fSD rrrrasurn ojthe Perron r•ee-ovvy e7civnries wabin the nurtra <br /> C=Carrepasite G=Grab <br /> LC.S-nreosure ojdie peraw recovery of the Luboraku7+Control Spike(LG:Sj <br /> .I ltat all Hao V Le, Laboratory Director DLR-Detection Limit jor the Pcrrpase n/Reporting. F. mptiaaol sample. <br /> wall-ires or inrerfcreriecev my resit&iu higher deieclian limits <br /> D <br /> Cil <br /> M <br /> w <br /> t_n <br /> EPef-£mirontnrntaiProlrctiar. en bfelhad. SM�SYantGtrd>1lethorlforE.rrrrrrirrniionoJiYttlerlYcuterrrtlerldrliFd. "'---- - - - <br /> Page I of I <br /> 545 E. Cleveland St. Suite A Stockton, CA 95204 Tal.: (209) 482.0892 Fax, 12041 4SP-7qqr-; <br />