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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Dentin Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr., Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose,CA 95112-1105 ReportNumber: IUI1062 Received: 09/13/11 <br /> Attention: Lorin King <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit MDL Result Factor Extracted Analyzed Qualifiers <br /> Sample ID: IUI1062-19(MW-21 -Water) Sampled:09/09/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 82608 1111489 0.50 0.28 13 1 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 8260B 1111489 0.50 0.25 ND 1 9/14/2011 9/15/2011 <br /> Toluene EPA 8260B 1111489 0.50 0.36 1.1 1 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 8260B 1111489 1.0 0.90 2.6 1 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82608 1111489 1.0 0.25 4.5 1 9/14/2011 9/15/2011 <br /> Ethyl tent-Butyl Ether(ETBE) EPA 8260B 1111489 1.0 0.28 0.75 1 9/14/2011 9/15/2011 J <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1111489 1.0 0.32 56 1 9/14/2011 9/15/2011 <br /> tert-Butanol(TBA) EPA 8260B 1111489 10 6.5 940 1 9/14/2011 9/15/2011 <br /> Surrogate:4-Bromofluorobenzene(80-110%) 101 % <br /> Surrogate:Dibromoffuorometharte(80-120916) 106% - <br /> Surrogate: Toluene-d8(80-1200) 106% <br /> Sample ID: IU11062-20(MW-22-Water) Sampled: 09/09/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 8260B 1111489 0.50 0.28 2.8 1 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 82606 1111489 0.50 0.25 1.6 1 9/14/2011 9/15/2011 <br /> Toluene EPA 82608 1111489 0.50 0.36 1.8 1 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 8260B 11I1489 1.0 0.90 4.9 1 9/14/2011 9/15/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 1111489 1.0 0.32 33 1 9/14/2011 9/15/2011 <br /> tert-Butanol(TBA) EPA 82608 1111489 10 6.5 730 1 9/14/2011 9/15/2011 <br /> Surrogate:4-Bromofluorobenzene(80-120%) 117% <br /> Surrogate:Dibromofluoromethane(80-120%) 103% <br /> Surrogate: Toluene-d8(80-1200) 103% <br /> Sample ID: IU11062-21 (MW-24-Water) Sampled:09/09/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 82608 1111489 25 14 4200 50 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 92606 1111489 25 12 320 50 9/14/2011 9/15/2011 <br /> Toluene EPA 8260B 1111489 25 18 78 50 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 8260B 1111489 50 45 56 50 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DUPE) EPA 82608 11I1489 50 12 25 50 9/14/2011 9/15/2011 J <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 1111489 50 16 140 50 9/14/2011 9/152011 <br /> tert-Butanol(TBA) EPA 82608 1111489 500 320 ND 50 9/142011 9/152011 <br /> Surrogate: 4-Bromofluorobenzene(80-120%) 99% <br /> Surrogate:Dibromofluoromethane(80-120516) 101 % <br /> Surrogate: Toluene-d8(80-110%) 105% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, <br /> except in full,without written permission from TestAmerica. 1 UI1061 <Page 21 of 67> <br />