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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Dentin Avenue.Suite 100, 6vine,CA 92614(949)261-1022 Pas-(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr.,Stockton,CA � � <br /> 1680 Rogers Avenue Sampled: 09/07/11.09/09/11 <br /> San Jose,CA 95112-1105 ReportNumber: IU11062 Received: 09/13/11 <br /> Attention: Lorin King <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit MDL Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUI1062-34(MW-38-Water) Sampled:09/09/11 <br /> Reporting Units: ug/1 <br /> Benzene EPA 8260B 1111489 0.50 0.28 ND 1 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 8260B 1111489 0.50 0.25 ND 1 9/14/2011 9/15/2011 <br /> Toluene EPA 8260B 1111489 0.50 0.36 ND 1 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 82608 1111489 1.0 0.90 ND 1 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82606 1111489 1.0 0.25 ND 1 9/14/2011 9/15/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 1111489 1.0 0.28 ND 1 9/14/2011 9/15/2011 <br /> Methyl-cert-butyl Ether(MTBE) EPA 8260B 1111489 1.0 0.32 5.2 1 9/14/2011 9/15/2011 <br /> Cert-Amyl Methyl Ether(TAME) EPA 82608 1111489 L0 0.33 ND 1 9/14/2011 9/15/2011 <br /> tert-Butanol(TBA) EPA 8260B 1111489 10 6.5 ND 1 9/14/2011 9/15/2011 <br /> Surrogate: 4-Bromofluorobenzene(80-120%) 106% <br /> Surrogate:Dibromofluoromethane(80-120%) 106% <br /> Surrogate., Toluene-d8(80-1200%) 106% <br /> Sample ID: IUI1062-35(MW-39-Water) Sampled:09/07/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 82608 1111493 5.0 2.8 770 10 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 8260B 1111493 5.0 2.5 18 10 9/14/2011 9/15/2011 <br /> Toluene EPA 8260B 1111493 5.0 3.6 28 10 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 8260B 1111493 10 9.0 33 10 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82608 1111493 10 2.5 ND 10 9/142011 9/15/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 82608 1111493 10 2.8 ND 10 9/14/2011 9/152011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 1111493 10 3.2 510 10 9/14/2011 9/15/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 1111493 10 3.3 ND 10 9/142011 9/15/2011 <br /> tert-Butanol(TBA) EPA 82608 1111493 100 65 ND 10 9/14/2011 9/15/2011 <br /> Surrogate: 4-Bromofluorobewzene(80-12001o) yT% <br /> Surrogate:Dibromofluoromethane(80-120%) 109% <br /> Surrogate: Toluene-d8(80-120%) /00% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results per(am only to the samples tested in the laboratory. This report shall not be reproduced, <br /> except In full,without written permisston from TesUmerlca. IU11062 <Page 26 of 67> <br />