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TestAmerica <br /> ]HE LEADER IN ENVIRONMENTAL TESTING 17461 Dedan Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Faxt(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr., Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose,CA 95112-1105 ReportNumber. IUI1062 Received: 09/13/11 <br /> Attention: Lorin King <br /> METHOD BLANK/QC DATA <br /> VOLATILE FUEL HYDROCARBONS BY GC/MS (CA LUFT) <br /> Reporting Spike Source %REC I2111) Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch: 1111329 Extracted:09/13/11 <br /> Blank Analyzed:09/1312011 (1111329-BLKI) <br /> Volatile Fuel Hydrocarbons(C4-C12) ND 50 ugA <br /> Surrogate:Dibromofluoromethane 24.2 u9/1 15.0 97 80-120 <br /> Surrogate.: Toluene-d8 24.1 149/1 25.0 97 80-120 <br /> Surrogate:4-Bromofluorobenzene 24.1 ug/I 25.0 97 80-120 <br /> LCS Analyzed:09/13/2011 (1111329-BS2) <br /> Volatile Fuel Hydrocarbons(424-C12) 410 50 ug/I 500 82 55-130 <br /> Surrogate:Dibromofluoromethane 231 u9/1 25.0 93 80-120 <br /> Surrogate: Toluene-d8 26.2 49/1 25,0 105 80-120 <br /> Surrogate:4-Bromofluorobenzene 13.6 149/1 25.0 95 80-120 <br /> Matrix Spike Analyzed:09/13/2011 (1111329-MSI) Source: IU10857-01 <br /> Volatile Fuel Hydrocarbons(C4-C12) 1350 50 ug/I 1720 735 35 50-145 M2 <br /> Surrogate:Dibromofluoromethane 23.9 ug/1 25.0 95 80-120 <br /> Surrogate: Toluene-d8 24.6 u9/1 25.0 99 80-120 <br /> Surrogate:4-Bromofluorobenzene 25,0 u9/1 25.0 100 80-120 <br /> Matrix Spike Dup Analyzed:09/13/2011 (1111329-MSDI) Source:IU10857-01 <br /> Volatile Fuel Hydrocarbons(C4-C12) 1410 50 ug/I 1720 735 39 50-145 5 20 M2 <br /> .Surrogate:Dibromofluoromethane 23.2 119/1 15.0 93 80-120 <br /> Surrogate:Toluene-d8 25.2 49/1 25.0 101 80-120 <br /> Surrogate:4-Bromofluorobenzene 25.4 u9/1 25.0 102 80-120 <br /> Batch: 1111489 Extracted:09/14/11 <br /> Blank Analyzed:09/14/2011 (1111489-BLKI) <br /> Volatile Fuel Hydrocarbons(C4-C12) ND 50 ug/I <br /> Surrogate:Dtbromo luoromethane 28.4 119/1 25.0 114 80-120 <br /> Surrogate:Toluene-d8 25.7 149/1 25.0 103 80-120 <br /> Surrogate:4-Bromofluorobenzene 24.9 249/1 25.0 100 80-120 <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results penam only to the samples tested in the laboratory. This report shall not be reproduced, <br /> except in full,without written permission from TestAmerica I UI1062 <page 31 of 67> <br />