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TestAmerica <br /> I"HE LEADER IN ENVIRGNt.IENTAL I"ESTING 17461 Derian Avenue,Suite 100, Irvine,CA 92614(949)261-1022 Fax'.(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose,CA 95112-1105 ReportNumber: IU11062 Received: 09/13/11 <br /> Attention: Lorin King <br /> VOLATILE ORGANICS by GC/MS (EPA 503011/826013) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch: 1111489 Extracted: 09/14/11 <br /> Matrix Spike Analyzed:09/14/2011 (1111489-MSI) Source: IU11062-13 <br /> Di-isopropyl Ether(DIPE) 45.5 1.0 ug/I 25.0 17.5 112 60-140 <br /> Ethyl tert-Butyl Ether(ETBE) 28.4 1.0 upfl 25.0 ND 113 60-135 <br /> Ethyl teri-Butyl Ether(ETRE) 28.4 1.0 ugA 25.0 ND 113 60-135 <br /> Methyl-tert-butyl Ether(MTBE) 26.6 1.0 ugfl 25.0 ND 106 55-145 <br /> Methyl-ten-butyl Ether(MTBE) 26.6 1.0 ugA 25.0 ND 106 55-145 <br /> Methyl-tert-butyl Ether(MTBE) 26.6 1.0 ug/I 25.0 ND 106 55-145 <br /> Methyl-tert-butyl Ether(MTBE) 26.6 1.0 ugA 25.0 ND 106 55-145 <br /> cert-Amyl Methyl Ether(TAME) 28.8 1.0 ugA 25.0 ND 115 60-140 <br /> ten-Butanol(TBA) 145 10 ugA 125 ND 116 65-140 <br /> tert-Butanol(TBA) 145 10 ug/I 125 ND 116 65-140 <br /> ten-Butanol(TBA) 145 10 ugA 125 ND 116 65-140 <br /> tert-Butanol(TBA) 145 10 ugA 125 ND 116 65-140 <br /> Surrogate:4-Bromofluorobenzene 15.6 ug/1 25.0 101 80-110 <br /> Surrogate:4-Bromofluorobenzene 25.6 ug/1 25.0 102 80-120 <br /> Surrogate:4-Bromofluorobenzene 15.6 119/1 25.0 102 80-120 <br /> Surrogate:4-Bromofluorobenzene 25.6 u9/1 25.0 102 80-120 <br /> Surrogate:4-Bromofluorobeuene 25.6 u9/1 25.0 102 80-120 <br /> Surrogate:Dibromofluoromethane 26.5 149/1 25.0 106 80-120 <br /> Surrogate:Dibromofluoromethane 26.5 ug/l 25.0 106 80-120 <br /> Surrogate:Dibromofluoromethane 26.5 u9/1 25.0 106 80-120 <br /> Surrogate:Dibromofluoromethane 26.5 u9/1 25.0 106 80-120 <br /> Surrogate:Dibromofluoromethane 26.5 u9/1 25.0 106 80-120 <br /> Surrogate: Toluene-dB 26.7 u9/1 15.0 107 80-120 <br /> Surrogate:Toluene-d8 26.7 u9/1 25.0 107 80-120 <br /> Surrogate:Toluene-d8 26.7 u9/1 25.0 107 80-120 <br /> Surrogate:Toluene-d8 26.7 u9/1 25.0 107 80-120 <br /> Surrogate:Toluene-d8 16.7 ug/l 25.0 107 80-120 <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced. <br /> except in full,without written permission from TestAmerica. /U/1062 <Page 45 of 67> <br />