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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL ILSII NL 17461 Derian Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07111-09/09/11 <br /> San Jose,CA 95112-1105 ReportNumber: IU11062 Received: 09/13/11 <br /> Attention: Lorin King <br /> METHOD BLANK/QC DATA <br /> VOLATILE ORGANICS by GUMS (EPA 5030B/8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch: 1111495 Extracted:09/14/11 <br /> Matrix Spike Dup Analyzed:09/14/2011 (1111495-MSDI) Source:IU11062-04 <br /> o-Xylene 29.1 0.50 ug/I 25.0 ND 117 65-125 0.6 20 <br /> o-Xylene 29.1 0.50 ug/I 25.0 ND 117 65-125 0.6 20 <br /> o-Xylene 29.1 0.50 ug/I 25.0 ND 117 65-125 0.6 20 <br /> Xylenes,Total 87.1 1.0 ug/1 75.0 ND 116 60-130 0.9 20 <br /> Xylenes,Total 87.1 1.0 ug/1 75.0 ND 116 60-130 0.9 20 <br /> Xylenes,Total 87.1 1.0 no 75.0 ND 116 60-130 0.9 20 <br /> Di-isopropyl Ether(DIPE) 25.3 1.0 ugA 25.0 ND 101 60-140 3 25 <br /> Di-isopropyl Ether(DIPE) 25.3 1.0 ugA 25.0 ND 101 60-140 3 25 <br /> MethyMert-butyl Ether(MTBE) 24.4 1.0 ug/I 25.0 ND 98 55-145 0.8 25 <br /> Methyl-ten-butyl Ether(MTBE) 24.4 1.0 ugA 25.0 ND 98 55-145 0.8 25 <br /> Methyl-ten-butyl Ether(MTBE) 24.4 1.0 ug/I 25.0 ND 98 55-145 0.8 25 <br /> ten-Amyl Methyl Ether(TAME) 26.0 1.0 ug/I 25.0 ND 104 60-140 0.5 30 <br /> ten-Butanol(TBA) 165 10 ugA 125 ND 132 65-140 2 25 <br /> ten-Butanol(TBA) 165 10 ugA 125 ND 132 65-140 2 25 <br /> Surrogate:4-Bromofluorobemene 24.4 ug/1 25.0 98 80-120 <br /> Surrogate:4-Bromofluorobenzene 24.4 119/1 25.0 98 80-120 <br /> Surrogate:4-Bromofluorobenzene 24.4 119/1 25.0 98 80-120 <br /> Surrogate:Dibromofluoromethane 23.8 u9/1 25.0 95 80-120 <br /> Surrogate:Dibromofluoromethane 23.8 ug/l 25.0 95 80-120 <br /> Surrogate:Dibromofluoromethane 23.8 119/1 25.0 95 80-120 <br /> Surrogate:Toluene-d8 15.6 u9/1 25.0 102 80-/20 <br /> Surrogate:Toluene-d8 25.6 u9/1 25.0 /02 80-120 <br /> Surrogate:Toluene-d8 25.6 119/1 15.0 102 80-/20 <br /> Batch: 1111631 Extracted:09/15/11 <br /> Blank Analyzed:09/15/2011 (1111631-BLKI) <br /> Benzene ND 0.50 ug/I <br /> Benzene ND 0.50 ugA <br /> Benzene ND 0.50 ugA <br /> Benzene ND 0.50 ugA <br /> Benzene ND 0.50 ugA <br /> Ethylbenzene ND 0.50 ugA <br /> Ethylbenzene ND 0.50 ugA <br /> Ethylbenzene ND 0.50 ugA <br /> Ethylbenzene ND 0.50 ugA <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, <br /> except in full,without written permission from TestAmerica. 1U11062 <Page 57 of 6h <br />