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TestAmeriaa <br /> 17461 Ded.Av..e..SuWte 100, Irvine,CA 92614(949)261-1022 Fm:(949)260-3297 <br /> THE LEADER IN ENVIRONMENTAL TESTING <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA Sampled: 03/30/11-03/31/11 <br /> 5900 Hollis St,Suite A <br /> Emeryville,CA 94608 ReportNumber: IUD0117 Received: 04/02/11 <br /> Attention: Aubrey Coot <br /> METHOD BLANK/QC DATA <br /> VOLATILE FUEL HYDROCARBONS BY GC/MS(CA LUFT) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch:11DO429 Extracted:04/05/11 <br /> Blank Analyzed:04/05/2011(11D0429-BLKI) <br /> Volatile Fuel Hydrocarbons(C4-C12) ND 10 mg/kg <br /> Surrogate:Dibromofluaromethane 1.37 mg/kg 2.50 95 55-140 <br /> Surrogate:Toluene-d8 2.41 mg/kg 2.50 96 60-140 <br /> Surrogate:4-Bromofluorobenzene 2.40 mg/kg 2.50 96 65-140 <br /> LCS Analyzed:04/05/2011(11D0429-BS2) MNR <br /> Volatile Fuel Hydrocarbons(C4-C12) 61.2 10 mg/kg 50.0 122 60-130 <br /> Surrogate:Dibromofluoromethane 2.51 mg/kg 2.50 100 55-140 <br /> Surrogate:Toluene-& 250 mg/kg 2.50 100 60-140 <br /> Surrogate:.4-Bromofluorobenzene 2.48 mg/kg 2.50 99 65-140 <br /> LCS Dup Analyzed:04/05/2011(11D0429-BSD2) <br /> Volatile Fuel Hydrocarbons(C4-Cl2) 61.1 10 mg/kg 50.0 122 60-130 0.3 25 <br /> Surrogate:Dibromofluoromethane 2.43 mg/kg 2.50 97 55-140 <br /> Surrogate:Toluene-d8 1.49 mg/kg 1.50 99 60-140 <br /> Surrogate:4-Bromofluorobemene 1.47 mg/kg 2.50 99 65-140 <br /> Batch: 11D0443 Extracted:04/05/11 <br /> Blank Analyzed:04/05/2011(11D0443-BLKI) _ <br /> Volatile Fuel Hydrocarbons(C4-C 12) ND 0.20 mg/kg <br /> Surrogate:Dibromofluoromethane 0.0524 mg/kg 0.0500 105 80-125 <br /> Surrogate:Toluene-d8 0.0509 mg/kg 0.0500 102 80-120 <br /> Surrogate:4-Bromofluorobemene 0.0481 mg/kg 0.0500 96 80-120 <br /> LCS Analyzed:04/052011(11D0443-BS2) <br /> Volatile Fuel Hydrocarbons(C4-C12) 1.13 0.20 mg/kg 1.00 113 60-135 <br /> Surrogate:Dibromofluoromethane 0.0521 mg/kg 0.0500 104 80-125 <br /> Surrogate:Toluene-0 0.0513 mg/kg 0.0500 103 80-120 <br /> Surrogate:4-Bromofluorobenzene 0.0496 mg/kg 0.0500 99 80-110 <br /> TestAmerica Irvine <br /> Pat Abe For Philip Sanelle <br /> Project Manager <br /> . The results pertain only to the rumples rested in the/abawrory. This reporr.rha!l not be reproduced, IUD0717 <page I2 Of 23> <br /> except in full,without written permission from TeslAmericu. <br />