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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Dmian Avenue.Suite 100, 1,ine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA i �- <br /> 5900 Hollis St.,Suite A Sampled: 04/06/11-04107/11 <br /> Emeryville,CA 94608 Report Number: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool <br /> VOLATILE FUEL HYDROCARBONS BY GC/MS (CA LUFT) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0863-01(AS-22-5-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11D1531 0.20 0.28 0.992 4/13/2011 4/132011 <br /> Surrogate:Dibromofluoromethane(80-12501o) 106% <br /> Surrogate: Toluene-d8(80-110016) 106% <br /> Surrogate:4-Bromofluorobenzene(80-120%) 90% <br /> Sample ID:IUD0863-05(AS-21-5-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS I ID1513 10 180 101 4/13/2011 4/142011 <br /> Surrogate:Dibromofluoromethane(55-140%) 96% <br /> Surrogate: Toluene-d8(60-1409,.) 97% <br /> Surrogate:4-Bromofluorobenzene(65-140%) 106% <br /> Sample ID:IUD0863-06(AS-21-10-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11 D1531 1.0 9.6 5.1 4/13/2011 4/13/2011 <br /> Surrogate:Dibromofluoromethane(80-12591) 103% <br /> Surrogate: Toluene-d8(80-120%) 105% <br /> Surrogate:4-Bromofluorobemene(80-120%) 100% <br /> Sample ID:IUD0863-07(AS-21-15-Sol]) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS IID1531 0.20 3.7 0.98 4/13/2011 4/132011 <br /> Surrogate:Dibronut luoromethane(80-11501.) 107% <br /> Surrogate:Toluene-d8(80-120%) 105% <br /> Surrogate:4-Bromofluorobenzene(80-110%) 102% <br /> Sample ID:IUD0863-09(AS-20-5-Sol]) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C 12) TPH byGC/MS IID1719 0.20 ND 0.99 4/14/2011 4/142011 <br /> Surrogate:Dibromofluoromethane(80-12501o) 110% <br /> Surrogate:Toluene-d8(80-120%) 105% <br /> Surrogate:4-Bromofluorobenzene(80-1201o) 97% <br /> Sample ID:IUD0863-10(AS-20-10-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS IID1531 0.97 14 4.85 4/13/2011 4/14/2011 <br /> Surrogate:Dibromofluoromethane(80-125%) 106% <br /> Surrogate: Toluene-d8(80-120a/a) 106% <br /> Surrogate:4-Bromofluorobenzene(80-120%) 107% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The reaulls pertain only to the samples tested in the laboratory. This report shall not be reproduced, (lID0863 < <br /> exceptIn full,without written permission from Temmerim. Page 5 0.f 37> <br />