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TABLET <br /> Page 3 of 3 <br /> SOIL ANALYTICAL DATA <br /> SHELL STOCKTON TERMINAL <br /> 3515 NAVY DRIVE,STOCKTON,CALIFORNIA <br /> Sample Depth Ethyl- Total <br /> ID Date (fbg) TPHg TPHd Benzene Toluene benzeneXylenes MTBE TBA DIPE ETRE TAME <br /> AS-22-5 4/6/2011 5 0.28 17a 0.0032 <0.00099 0.0016 <0.0020 <0.0020 <0.020 <0.0020 <0.0020 <0.0020 <br /> Notes: <br /> All results in milligrams per kilogram(mg/kg)unless otherwise indicated. <br /> fbg=Feet below grade <br /> TPHg=Total petroleum hydrocarbons as gasoline analyzed by EPA Method 8260B <br /> TPHd=Total petroleum hydrocarbons as diesel,analyzed by EPA Method 8260B <br /> Benzene,toluene,ethylbenzene,and xylenes analyzed by EPA Method 8260B <br /> MTBE=Methyl tertiary butyl ether analyzed by EPA Method 8260B <br /> TBA=Tertiary butyl alcohol analyzed by EPA Method 8260B <br /> DIPE=Di-isopropyl ether analyzed by EPA Method 8260B <br /> ETBE=Ethyl tertiary butyl ether analyzed by EPA Method 8260B <br /> TAME=Tertiary amyl methyl ether analyzed by EPA Method 8260B <br /> <x=Not detected at reporting limit x <br /> a=Hydrocarbon result partly due to individual peak(s)in the quantitation range <br /> c=Calibration verification recovery was above the method control limit for this analyte. Analyte not detected, <br /> data not impacted. <br /> d=Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the acceptance limits. <br /> Analyte not detected,data not impacted. <br /> e=The MS and/or MSD were above the acceptance limits due to sample matrix interference. See Blank Spike(LCS). <br /> f=Reporting limit raised due to sample matrix effects. <br /> g=The MS and/or MSD were above the acceptance limits. See Blank Spike(LCS). <br /> h=The RPD exceeded the method control limit due to sample matrix effects. The individual analyte QA/QC recoveries, <br /> however,were within acceptance limits. <br /> i=The RPD exceeded the acceptance limit due to sample matrix effects. <br /> j=The MS and/or MSD were below the acceptance limits. See Blank Spike(LCS). <br /> CRA 241r (31) <br />