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TestAmerica <br /> THE LEADER. IN ENV IR014 MENIAL TESTING 17461 Dmian Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 03/23/11 <br /> Emeryville,CA 94608 ReportNumber: IUC2973 Received: 03/29/11 <br /> Attention: Aubrey Cool _ <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUC2973-01(AS-5-5-Soil) <br /> Reporting Units: mgAtg <br /> Benzene EPA 82606 11D0429 0.050 0.40 99.9 4/5/2011 4/6/2011 <br /> Ethyibenzene EPA 8260E 1ID0429 0.050 1.6 99.9 4/52011 4/6/2011 <br /> Toluene EPA 8260B 11D0429 0.050 0.15 99.9 4/52011 4/62011 <br /> Xylenes,Total EPA 8260B I ID0429 0.10 6.4 99.9 4/52011 4/62011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11DO429 0.10 ND 99.9 4/5/2011 4/62011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 1 ID0429 0.10 ND 99.9 4/5/2011 4/62011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B I ID0429 0.10 ND 99.9 4/5/2011 4/62011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D0429 0.10 ND 99.9 4/5/2011 4/62011 C <br /> tert-Butanol(TBA) EPA 8260B I ID0429 1.0 ND 99.9 4/52011 4/62011 <br /> Surrogate:4-Bromofluorobenzene(65-140%) 92% <br /> Surrogate:Dibromofluoromethane(55-140%) 90% <br /> Surrogate: Toluene-d8(60-140%) 91% <br /> Sample ID:IUC2973-02(AS-5-10-Soil) <br /> Reporting Units: mglkg <br /> Benzene EPA 8260B I ID0429 0.20 1.6 399 4/52011 4/5/2011 <br /> Ethylbenzene EPA 8260B IID0429 0.20 9.5 399 4/5/2011 4152011 <br /> Toluene EPA 8260B 11DO429 0.20 0.42 399 4/52011 4/52011 <br /> Xylenes,Total EPA 8260B I ID0429 0.40 45 399 4/5/2011 4/52011 <br /> Di-isopropyl Ether(RIPE) EPA 8260E 11D0429 0.40 ND 399 4/52011 4/52011 <br /> Ethyl tert-Butyl Ether(ETRE) EPA 8260B 11DO429 0.40 ND 399 4/5/2011 4/52011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 11D0429 0.40 ND 399 4/52011 4/52011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D0429 0.40 ND 399 4/52011 4/5/2011 C <br /> tert-Butanol(TBA) EPA 8260E 11D0429 4.0 ND 399 4/5/2011 4/52011 <br /> Surrogate:4-Bromofluorobemene(65-140%) 105% <br /> Surrogate:Dibromofluoromethane(55-140%) 86% <br /> Surrogate: Toluene-d8(60-140%) 96% <br /> TestAmerica Irvine <br /> Lena Davidkova For Philip Sanelle <br /> Project Manager <br /> The resul(s permin only to the sampler tested in the laboratory. This reportshall not be reproduced, 1UC2973 GPag¢4Of 11> <br /> esceptin full,without written permission from TestAmerica. <br />