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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite loo, Irvine,CA 92614(949)261-1022 Fax(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 03/29/11-03/30/11 <br /> Emeryville,CA 94608 Report Number: IUC3240 Received: 03/31/11 <br /> Attention: Aubrey Cool <br /> VOLATILE FUEL HYDROCARBONS BY GC/MS(CA LUFT) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted .Analyzed Qualifiers <br /> Sample ID:IUC3240-01(AS,3-5-Soil) Sampled:03/29/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 1ID0275 0.20 ND 0.996 4/4/2011 4/4/2011 <br /> Surrogate:Dibromofluoromethane(80-1250 - 100% <br /> Surrogate: Toluene-0(80-110%) 104% <br /> Surrogate:4-Bromofluorobenzene(80-12001o) 95% <br /> Sample ID:IUC3240-02(AS-3-10-Soil) Sampled:03/29/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-Cl2) TPH by GC/MS IID0275 0.20 1.9 0.996 4/4/2011 4/4/2011 <br /> Surrogate:Dibromofluoromethane(80-125%) 106% <br /> Surrogate:Toluene-d8(80420%) 104% <br /> Surrogate:4-Bromofluorobenzene(80-12051) 99% <br /> Sample ID:IUC3240-05(AS-2S-SoiD Sampled:03/29/11 <br /> Reporting Unics: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11DO275 0.20 1.7 0.996 4/4/2011 4/42011 <br /> Surrogate:Dibromofluoromethane(80-125516) 104% <br /> Surrogate:Toluene-d8(80-120%) 105% <br /> Surrogate:4-Bromofluorobenzene(80-120%) 100% <br /> Sample ID:IUC3240-06(AS-2-10-Soil) Sampled:03/29/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-Cl2) TPH by GC/MS l ID0429 50 900 499 4/5/2011 4/62011 <br /> Surrogate:Dibromofluoromethane(55-140%) 68% Z? <br /> Surrogate:Toluene-d8(60-140%) 80% Z3 <br /> Surrogate:4-Bromofluorobenzene(65-14051) 104% Z3 <br /> Sample ID:IUC3240-09(AS-19-5-Soil) Sampled:03/30/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11D0617 0.20 ND 0.986 4/6/2011 4/6/2011 <br /> Surrogate:Dibromofluoromethane(80-125%) 103% <br /> Surrogate: Toluene-d8(80-120%) 101% <br /> Surrogate:4-Bromof7uorobenzene(80-120%) 96% <br /> Sample ID:IUC3240-10(AS-19-10-Soil) Sampled:03/30/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS l ID0443 0.20 ND 0.977 4/52011 4/6/2011 <br /> Surrogate:Dibromofluoromethane(80-125a/o) 104% <br /> Surrogate:Toluene-d8(80-12091o) 103% <br /> Surrogate:4-Bromofluorobenzene(80-120%) 94% <br /> TestAmerica Irvine <br /> Lena Davidkova For Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested In the laboratary. This reparlshnll not be reproduced, <br /> excepHn fu/l,without wrilam permissian from raimmerlca. IUC3240 <Page 3 of 23> <br />