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L <br /> TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, Wine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St,Suite A Sampled: 03/29/11-03/30111 <br /> Emeryville,CA 94608 ReportNumber: IUC3240 Received: 03/31/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID: IIJC3240-13(AS-18-5-Soil) Sampled:03/30/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260E IID0275 0.0010 0.0098 0.996 4/4/2011 4/5/2011 <br /> Ethylbenzene EPA 8260E IID0275 0.0010 ND 0.996 4/4/2011 4/5/2011 <br /> Toluene EPA 82608 11D0275 0.0010 ND 0.996 4/4/2011 4/5/2011 <br /> Xylenes,Total EPA 8260B 11D0275 0.0020 ND 0.996 4/4/2011 4/5/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11D0275 0.0020 ND 0.996 4/4/2011 4/5/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 82608 I ID0275 0.0020 ND 0.996 4/42011 4/52011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11D0275 0.0020 0.078 0.996 4/42011 4/52011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260E 11D0275 0.0020 ND 0.996 4/42011 4/52011 C <br /> tert-Butanol(TBA) EPA 8260B 11D0275 0.020 0.039 0.996 4/4/2011 4/52011 <br /> Surrogate:4-Bromofluorobemene(80-120%) 96% <br /> Surrogate:Dibromofluoromethane(80-12501o) 102% <br /> Surrogate: Toluene-d8(80-12091) 104% <br /> Sample ID:IUC3240-14(AS-18-10-Soil) Sampled:03/30/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D0275 0.0025 0.084 2.48 4/4/2011 4/5/2011 <br /> Ethylbenzene EPA 8260B I ID0275 0.0025 0.0029 2.48 4/42011 4/52011 <br /> Toluene EPA 8260B 11D0275 0.0025 ND 2.48 4/4/2011 4/52011 <br /> Xylenes,Total EPA 8260E I1D0275 0.0050 ND 2.48 4/42011 4152011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B I ID0275 0.0050 ND 2.48 4/4/2011 4/52011 <br /> Ethyl tert-Butyl Ether(ETRE) EPA 8260B I ID0275 0.0050 ND 2.48 4/42011 4/52011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B I ID0275 0.0050 0.47 2.48 4/4/2011 4/5/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D0275 0.0050 ND 2.48 4/4/2011 4/52011 C <br /> tert-Butanol(TBA) EPA 8260B I ID0275 0.050 0.26 2.48 4/42011 4/52011 <br /> Surrogate:4-Bromofluorobemene(80-120%) 104% <br /> Surrogate:Dibromofluoromethane(80-125%) 102% <br /> Surrogate:Toluene-&(80-12091) 105% <br /> TestAmerica Irvine <br /> Lena Davidkova For Philip Sanelle <br /> Project Manager <br /> The sesa((s pertain only to the samples tested in the laboratory. This report shall not be reproduced. IOC3240 <Pa e 8 0f 23> <br /> exceptInfull,without nvruientrennisslonfron,TestAmenca. g <br />