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Analy4is Report Lancaster Laboratories Page 3 of 3 Where quaality Is a science Qulity Control Summary Client Name ChevronTexaco Group Dumber 807990 Reported 05/29/02 at 08 43 AM Blank 84 Surrogate Quality Control LCS 100 MS 97 MSD 93 Limits 61-127 Analysis Name UST-Unleaded Soils by 8260B Batch number D021401AB Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene 3821830 110 93 95 112 3821831 108 90 94 112 3821832 110 89 93 110 3821833 110 84 93 111 3821834 111 87 93 111 3821835 112 87 94 113 Blank 106 91 91 109 LCS 99 102 93 104 MS 103 95 97 109 MSD 99 92 92 107 Limits 80-120 80-120 81-117 74-121 Analysis Name UST-Unleaded Soils by 8260E Batch number D021411AA Dibromofluoromethane 1,2-Dxchloroethane-d4 Toluene-d8 4-Bromofluorobenzene 21836 111 96 94 107 ank ank 106 91 91 109 CS 109 103 92 110 MS 109 95 99 110 MSD 102 92 97 110 Limits 80-120 80-120 81-117 74-121 Analysis Name UST-Unleaded Soils by 8260E Batch number D021411AB Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene 3821837 105 86 93 102 3821838 106 87 101 110 3821839 107 88 97 108 3821840 112 Be 100 111 3821841 107 86 97 108 3821842 116 90 97 115 3821843 110 86 98 113 3821844 117 89 101 117 3821845 114 86 101 118 3821846 115 89 98 120 3821847 114 85 100 119 3821848 115 91 100 120 Blank 105 99 97 109 LCS 109 103 92 110 MS 109 95 99 110 MSD 102 92 97 110 Limats 80-120 80-120 81-117 74-121 *-Outside of specification 1) The result for one or both determinations was less than five times the LOQ The background result was more than four times the spike added Lancaster Laboratories Inc M E M B E R 2425 New Holland Pike Box 12425 La � Lancaster PA 17605 2425 717 656 2300 Fax 717 656 2681 2216 Rev 9/11100