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� -- � e ti.�t4ti• v � 1 ) e . +w. 1 aY ac4�«.Ni�u�A 1A.:xiwi�� ' ASSOCIATED LABORATORIES QA REPORT FORM(MS/MSD) ' C Sample LR 91717-344715 QC#042302W ' Matrix WATER Prep Date 04/23/02 ' Analysis Date 04/24/02 ' Lab ID#'s in Batch LR 91717, 91693,91711,91686,91618,91700,91660,91699,91621,91516,91697,91696, LR 91596, 91698,91674 MATRIX SPIKE I MATRIX SPIKE DUPLICATE RESULT REPORTING UNITS= mg/L Sample Spike Matrix Matrix %Ree %Ree TEST Method Result ND Added Spike Spike Dup MS MSD RPD Arsenic 200 7/6010 0 021 0 1 0 103 0 101 820 800 20 Selenium 2007 0010 0 016 01 0 099 0 102 830 860 30 ' Thallium 2007 , 6010 0 019 01 0 118 0 119 990 1000 08 Lead 200 7 1 6010 0 010 02 0 186 0 184 880 870 l 1 ' timony 2007 6010 0 042 1 0 1 000 0 980 958 93 8 20 anum 200 7/6010 0 097 1 0 1 110 1 080 1013 983 27 Beryllium 2007 1 6010 0 005 U 10 0 920 0 910 920 91 0 1 1 Cadmium 2007 / 6010 0 005 U 1 0 0 990 0 970 990 970 20 Chromium 200 7/6010 0 010 U 1 0 0 990 0 970 990 970 20 Cobalt 2007 6010 0 005 U 1 0 0 960 0 940 960 940 2 1 ICopper 2007/6010 0 010 U 10 0 980 0 960 980 960 2 1 Molybdenum 200716010 0 031 to 1 000 1 000 969 969 00 Nickel 200 7 6010 0 015 U 1 0 0 970 0 950 970 950 2 1 Silver 200 7/6010 0 005 U 04 0 360 0 360 900 900 00 Vanadium 200 7/6010 0 036 10 1 030 1 010 994 974 20 Zinc 200 7/6010 0 071 1 0 1 030 1 000 959 929 30 Aluminum 200 7/6010 2 270 1 0 3 000 3 000 730 730 00 Iron 2007 ,6010 2 740 1 0 3 530 3 500 790 760 09 Manganese 200 7/6010 0 080 1 0 1 060 1 030 980 950 29 oron 200 7 /6010 0 221 1 0 1 190 1 160 969 939 26 I *=Outside QC limits,due to matrix Interference NC=Not Calculated ND= 'U"-Not Detected IV,RDC LIMITS= 75 125 ' RPD=Relative Percent Difference of Matrix Spike and/Lfatrix Spike Diiplrcate RPD LIMITS =E20 %REC MS&MSD=Percent Recovery of Matrix Spike&Matrix Spoke Duplicate 4/26/2002 200 70423w I Page 1 of 2