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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> .Sample 138880-566793 <br /> Matrix WATER <br /> Prep Date October 25,2004 <br /> Analysis Date October 25, 2004 <br /> ID#'s in Batch LR 138880, 139015 <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units= mg/L <br /> Sample Spike Matrix Matrix %Rec %Ree <br /> Test Method Result Added Spike Spk.Dup MS MSD RPD <br /> TRPH 4181 ND 412 3 80 1 340 1 92 1 83 1 11 <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate %REC LIMITS = 70 - 130 <br /> �C-MS c&MSD=Percent Recovery ofMatnx Spike&Matrix Spike Duplicate IRPDLIMITS = 30 <br /> PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value Result True %Rec L.L:aut H.Limit <br /> ND 1560 1650 95 80% 120% <br /> Value=Preparation Blank value ND=Nod-Detected <br /> LCS Result=Lab Control Sample Result <br /> True=True Value of LCS <br /> L Limit/H Limit=LCS Control Limits <br /> • <br /> 10/29/2004 418 1 TRPH 1025 W <br />