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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> • QC Sample LR 58269-402 <br /> Matrix WATER <br /> Prep Date 08/25/00 <br /> Analysis Date 08/25/00-08/26/00 <br /> ID#'s in Batch LR 58269,58216, 58205,58239 <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units=ug/L <br /> Sample Spike Matrix Matrix %Ree %Ree <br /> Test Method Result Added S ike S ike Du MS MSD RPD <br /> TPH 8015M-G ND 400 413 387 1033 968 65 <br /> ND=Not Detected <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate %REC LIMITS = 70 - 130 <br /> %PEC-MS&MSD=Percent Recovery of Matrix Spike&Mamx Spike Duplicate !RPD LIMI7S = 30 <br /> PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value Result True %Ree L.Limit H.Limit <br /> ND 463 500 926 80% F 120% <br /> LCS Result=Lab Control Sample Result <br /> True= True Value of LCS <br /> L Limit/H Limit=LCS Control Limits <br /> 09/25/2000 8015g_tph_0825w] xls <br />