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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> QC Sample 153201-634253 <br /> Prep Date July 13, 2005 <br /> Analysis Date June 13, 2005 <br /> ID#'s in Batch LR 153123, 153172, 153201, 153406 _ <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units <br /> Sample Spike Matrix MatrixRec %Rec <br /> Test Method Result Added Spike Spk.DupE!/MS MSD RPD <br /> TRPH 4181 ND 412 330 3 60 80 87 9 <br /> RPD—Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate j;Y-16RECLIUMS = 70 - 130 <br /> %REC-MS&MSD=Percent Recovery ofMatrix Spike&Mainx Spike Duplicate D IIMM = 30 <br /> SARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value=Preparation Blank Value, ND=Not-Detected <br /> LCS Result=Lab Control Sample Result <br /> True=True Value of LCS <br /> L Limit/Hbinit=LCS Control Limits <br /> 7/14/2005 4181 TRPH 0613 Wl <br />