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' ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> 1 <br /> ample 144279-591408 <br />'1VIatnnx WATER <br />'Prep Date January 31,2005 <br /> Analysis Date January 31,2005 <br /> 1ID4's in Batch LR 144279, 144295, 144363 <br />'MATRIX SPIKE 1 MATRIX SPIKE DUPLICATE RESULT <br />'Reporting Units= mg/L <br /> Sample Spike Matrix Matrix %Rec %Rec <br /> iE Test Method Result Added Spike Spk.Dup MS MSD RPD <br /> TRPH 4181 ND 4 12 380 3 55 _]_ 92 86 7 <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate %REC LIMITS = 70 - 130 <br /> %REC-MS&MSD=Percent Recovery of Matrix Spike&Matrix Spike Duplicate RPD LIMITS = 30 <br /> PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value Result True %Rec L.Lmut H Limit <br /> ND 15 7 L 165 95 80% 120% <br />' Value=Preparation Blank Value ND=Not-Detected <br /> LCS Result=Lab Control Sample Result <br /> True= True Value ofLCS <br />' L Limit I HLimit=LCS Control Limits <br />' 21812005 4181 TRPH 0131 W <br />