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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> ample 145421-596926 <br />,Matrix WATER <br />,Prep Date February 16,2005 <br /> Analysis Date February 16,2005 <br /> 9D#'s in Batch LR 145114, 145115, 145116, 145117, 145118, 145125, 145137, 145418, 145419, 145420, <br /> LR 145421, 145130 <br />'MATRIX SPIKE 1 MATRIX SPIKE DUPLICATE RESULT <br />'Reporting Units= mg/L <br /> Sample Spike Matrix Matrix %Ree %Ree <br /> Test Method Result Added Spike Spk.Dup MS MSD RPD <br /> TRPH 4181 ND 412 440 460 107 112 4 <br /> 1 <br /> RPD=Relative Percent Difference of Matnx Spike and Matrix Spike Duplicate °Yo.RE'C LIMITS = 70 - 130 <br /> NC-MS&MSD=Percent Recovery of Matnx Spike&Matrix Spike Duplicate IRPI)LIMITS = 30 <br />'PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br />' Value Result True %Rec L.Lfmit H.Limit <br /> ND 177 165 107 80% 120% <br />'Value =Preparation Blank Value ND=Not-Detected <br /> LCS Result=Lab Control Sample Result <br /> True=True Value of LCS <br />'L Limit/HLimit=LCS Control Limits <br /> i <br /> 1 <br /> 2/23/2005 418 1 TRPH 0216 Wl <br />