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05/28/2003 13:36 209572' `5 GEO PAGE 03/20 <br /> GeoAnalytical Laboratories, Inc. <br /> 7405 KAnsas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax(209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# P14.3.11 Oxygenates Date: 5/28/03 <br /> Co. Pmect: Soil Sampling Card Lock) Stockton Bate Recd: 5/23/03 <br /> DonLee Pump jp g-� Date Started: - 5/27/03 <br /> P.O.Box 276 Date Completed5/27/03 <br /> Ceres CA 95307 PO# <br /> Date Sampled: 5/23/03 <br /> Sampler. R.Azevedo(Geo) <br /> Sample 10 Lab YD RL Method Analyte Results Units <br /> Soil Sample #4®2' P200865 10 8260B Methyl tent-butyl ether(MTBE) ND ug/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-I.9*0pyl ether(DIPS) ND <br /> 10 Ethyl Cert-butyl ether(ETBE) ND <br /> 10 ter.t-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dich0oroethane-d4 20 22-1. 110.50 66-133 <br /> 2-Brorno-1-cb1oropropzne 20 23.7 118.50 63.139 <br /> 4-Bromof iambenzene 20 19.4 97.00 64-136 <br /> Soil Sample #5 02' P200666 1.0 8260B Methyl Cert-butyl ether(MTBE) 38 µg/Kg <br /> 400 Ethanol NO <br /> 200 tert-Butanol ND <br /> 10 di-lsopropyl ether(D1PE) NTD <br /> 10 Ethyl tent-butyl ether(ETRE) ND <br /> 1.0 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit <br /> 1,2-DicbloroCthafte-d. 20 23.0 1150 66.133 <br /> 2-Bromo-l-chlomprnpane 20 27.0 135.110 63-139 <br /> 4-$romofiuorobenzene 20 1.9.0 95.00 64-136 <br /> Soil Sample #602' P200867 10 8260E Methyl tert-butyl.ether(MTBE) ND ug/Kg <br /> 400 Ethanol ND <br /> 200 tent-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 EtbyI tert-butyl ether(ETRE) ND <br /> 10 tert-Amy)methyl ether('TAME) ND <br /> surrogate A?nnt Spiked Amttt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d. 20 22.6 113.00 66-133 <br /> 2-13romo-1-chl6ropropanc 20 24.8 124.00 63.139 <br /> 4-Bromothioroben7ene 20 18.9 94.50 64-136 <br /> r . . II <br /> iar�'D'Ofrio <br /> Y c-- i��Donna Keller <br /> Chemist Certification # 3.157 Laboratory Director <br />