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JUN-02-2000 04 :20 PM DONLEE PUMP CO: 209 537 9598 P. 11 <br /> p <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS - - <br /> Report# P143-11 Date: 3/28/03 <br /> Date Rec'd: 5/23/03 <br /> DonLee Pump Co. Project: Soil Sampling-(Card Lock) Stockton Date Started: 5/27/03 <br /> P.O.Box 276 Date Completed0/27/03 <br /> Ceres CA 95307 PO# <br /> Date Sampled: 3/23/03 <br /> Sampler: R.Azevedo(Geo) <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> Suil Sample #5®2' P200866. 1.0 3550 LUFT Diesel 9.6 mg/kg <br /> Surrogate. Arent Spiked Arent Recavcrcd %Recovery QC Limit <br /> o-TPrphcnyl 1.00 0.91 91.0 70-130 <br /> Still Sample it 6 02' P200867 1.0 3550 LUFr Diesel ND n/Kg <br /> Surrogate Amnt Spiked Amnt Recovered °/Recovery Qt;:IArnit% <br /> o-Terphcnyl 1,00 0.82 82.0 70-130 <br /> Soil Sarnple 4 7®2' P200868 1.0 3550 1.UFT Diesel 31 mg/Kg <br /> SurroKate Amnt Spiked Amnt Recovered %Recovery QC Urrdt%u <br /> o-Terplie»yl 1.00 0.83 83.0 70-130 <br /> Snit Sample #802' P200869 10 3550 1;.U1'T Diesel 6100 mg/Kg <br /> Surrogate Arrant Spiked Amnr Recovered /,Recovery QC Unit% <br /> o-Tcrphcnyl 1.Q0 12.72 <br /> 272.0 70.130 <br /> *Flovaicd duc to high level of analyte in st-unple. <br /> reg8lry Merciadis Doraia Keller <br /> Chemist Certification # 1157 l,.aboratory Director <br />