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CALIFORNIA LABORATORY SERVICES <br /> p� �� g 03/10104 09 03 <br /> ENSR-Sacramento Project Former Unocal 5098,5606 CLcfWprake Ott e'N"ENAC0022 <br /> 10411 Old Placerville Rd,Suite 210 Project Number 06940-293-100 COC# 1,2,3,4 <br /> Sacramento,CA 95827-2508 Project Manager Ben I Henmgburg <br /> ' Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> ' Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch CN0180I-EPA 5030 Water MS <br /> ' Blank(CN01801-BLK1) Prepared&Analyzed 03/04/04 <br /> 1,3,5-TnmethyIbenzene ND 050 pg1L <br /> Vinyl chloride ND to <br /> Xylenes(total) ND to <br /> Di-isopropyl ether ND 050 <br /> Ethyl tert-butyl ether ND 050 <br /> tent-Amyl methyl ether ND 050 " <br /> Tert-butyl alcohol ND 50 °' <br /> Surrogate 12-Dichloroethane-d4 110 100 110 66-135 <br /> Surrogate Toluene-d8 986 100 986 72-115 <br /> INCS <br /> rogate 4-Bromofluorobenzene 987 100 987 73-115(CN01801-BSI) Prepared&Analyzed 03/04/04 <br /> Benzene 201 050 pg/L 200 100 60-135 <br />' Chlorobenzene 19 3 050 20 0 965 60-133 <br /> 1,1-Dichloroethene 235 050 200 118 42-150 <br /> Toluene 197 050 200 995 60-137 <br />' Tnehloroethene 201 050 200 100 62-140 <br /> Surrogate 1 2-Dichloroethane-d4 106 100 106 66-135 <br /> Surrogate Toluene-d8 102 100 102 71-115 <br /> Surrogate 4-Bromofluorobenzene 985 100 983 73-125 <br />' LCS Dup(CN01801-BSD1) Prepared& Analyzed 03/04/04 <br /> Benzene 202 050 pg/L 200 101 60-135 0 496 25 <br /> Chlorobenzene 193 0 50 20 1) 965 60-133 0 00 25 <br />' 1,1-Dichioroethene 23 6 050 200 118 42-150 0 425 25 <br /> Toluene 199 050 200 995 60-137 1 01 25 <br /> Trtchloroethene 202 050 200 101 62-140 0 496 25 <br />' Surrogate 12-Dichloroethane-d4 11 1 ;i 100 111 66-135 <br /> Surrogate Toluene-d8 102 10 0 102 72-125 <br /> Surrogate 4-Bromofluorobenzene 983 100 98 3 73-125 <br /> I <br /> I <br /> CA DOHS FLAP AccredrtationlRegtstratlon Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www californialab corn 916-638-7301 Fax 916-638-4510 <br />