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CALIFORNIA LABORATORY SERVICES <br /> ' 03/10/04 09 03 <br /> ' ENSR-Sacramento Project Former Unocal 5098,5606Q�c W��p'A, a ggto kt ccAA <br /> 10411 Ofd Placerville Rd,Suite 210 Project Number 06940-293-100 CLWorvk Ort�er 'CNC0022 <br /> Sacramento,CA 95$27-2508 Project Manager Ben 1 Hentngburg <br /> COC# 1,2,3,4 <br /> ' Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> ' Reporting Spike Source %REC RAD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch CN01912-PPA 5030 Water MS <br /> IBlank(CN01912-BLKI) Prepared&Analyzed 03/05/04 <br /> 1,3,5-Tnmethylbenzene ND 050 gg/L <br /> Vinyl chloride ND to " <br /> ' Xylenes(total) ND 10 " <br /> Di-isopropyl ether ND 050 <br /> Ethyl Cert-butyl ether ND 050 <br /> tert-Amyl methyl ether ND 050 " <br /> Tert-butyl alcohol ND 50 <br /> Surrogate 12-Dichloroethane-d4 909 100 909 66-135 <br /> Surrogate Toluene-& 9 79 100 979 71-125 <br /> Wurrogate 4-Bromofluorobemene 103 100 103 73-125 <br /> CS(CN01912-BSI) Prepared&Analyzed 03/05/04 <br /> Benzene 221 050 pglL 200 110 60-135 <br /> ' Chlorobenzene 217 050 200 108 60-133 <br /> 1 1-Dichloroethene 226 050 200 113 42-150 <br /> Toluene 221 050 200 110 60-137 <br /> Tnehloroethene 21 7 050 200 108 62-140 <br /> Surrogate 12-Dichloroethane-d4 904 100 904 66-135 <br /> Surrogate Toluene48 100 100 100 71-125 <br /> Surrogate 4-Bromofluorobenzene 102 100 102 73-115 <br /> LCS Dup(CN01912-ESDI) Prepared&Analyzed 03/05/04 <br /> Benzene 224 0 50 pg/L 200 112 60-135 135 25 <br /> Chlorobenzene 22 I 050 200 110 60-133 1 83 25 <br /> l I-Dichloroethene 23 1 050 200 116 42-150 2 19 25 <br /> Toluene 223 050 200 112 60-137 0 901 25 <br /> Trichloroethene 21 8 050 200 109 62-140 0 460 25 <br /> Surrogate 1 2-Dichloroethane-d4 902 „ 100 902 66-135 <br /> Surrogate Toluene-d8 9 91 100 991 71-115 <br /> Surrogate 4-Bromafluorobenzene 101 100 101 73-115 <br /> CA DOHS ELAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www californialab.com 916-638-7301 Fax 916-638-4510 <br />