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CALIFORNIA LABORATORY SERVICES <br /> 01/05/04 17 19 <br /> ENSR-Sacramento Project Former Unocal 5098,5606 CLSfW.AW69 2n'CML0881 <br /> 10411 Old Placerville Rd,Suite 210 Project Number 06940-293-100 COC# 1,2,3,4 <br /> Sacramento,CA 95827-2508 Project Manager Ben Henmgburg <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Reporting <br /> Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes <br /> ' MW-9(CML0881-08)Water Sampled 12/18/0315 21 Received 12/23/03 10 50 <br /> Xylenes(total) ND 10 kg1L I CA40209 12/31/03 12/31/03 EPA 8260B <br /> Di-isopropyl ether ND 050 " 01/02/04 " <br /> Ethyl tert-butyl ether ND 050 R " <br /> Tert-amyl methyl ether ND 0 50 " <br /> Tert-butyl alcohol ND so " <br /> Surrogate 1,2-Dichloroethane-d4 125% 66-135 12131103 <br /> Surrogate Toluene-& 980% 72-125 " <br /> Surrogate 4-Bromofluorobenzene 987% 73-125 " <br /> MW-10(CML0881-09)Water Sampled 12/18/03 17 15 Received 1223103 10 50 <br /> Acetone ND 10 µg/L 1 CL33026 12/30/03 12/30/03 EPA 8260B <br /> Benzene 36 050 " <br /> Wromobenzene ND 0 50 " <br /> mochloromethane ND 050 <br /> " <br /> 'l�romodtchloromethane ND 050 " <br /> Bromoform ND 050 " <br /> Bromomethane ND 10 " <br /> 2-Butanone ND 10 <br /> n-Butylbenzene ND 0 50 <br /> sec-Butylbenzene ND 050 " <br />' tert-Butylbenzene ND 0 50 " <br /> Carbon tetrachloride ND 050 " <br /> Chlorobenzene ND 050 " <br /> Chloroethane ND 050 <br />' Chloroform ND 0 50 <br /> Chloromethane ND 10 " <br /> o-Chlorotoluene ND 0 50 " <br /> p-Chlorotoluene ND 050 <br /> Dibromochloromethane ND 0 50 n " <br /> 1,2-Dtbromo-3-chloropropane ND 10 <br /> 1,2-Dibromoethane(EDB) ND 0 50 " <br /> Dâ–ºbromomethane ND 050 <br /> 1,2-Dichlorobenzene ND 050 " <br /> 1,3-Dichlorobenzene ND 0 50 " <br /> 1,4-13,chlorobenzene ND 0 5017 " <br /> e <br /> GA DOHS ELAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www californialab.com 916-638-7301 Fax 916-638-4510 <br />