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CALIFORNIA LABORATORY SERVICES <br /> 01/05/04 17 19 <br /> ENSR-Sacramento Project Former Unocal 5098,5606 ffir*A a Noce 1r,&L0881 <br /> ' 10411 Old Placerville Rd,Suite 210 Project Number 06940-293-100 GOC# 1,2,3,4 <br /> Sacramento,CA 95827-2508 Project Manager Ben Heningburg <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Reporting <br /> Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes <br /> MW-11(CML0881-10)Water Sampled 12/19/03 13 40 Received 12/23103 10 50 <br /> 1,2,4-Trichlorobenzene ND 50 µg/L 10 CA40209 12/31/03 12/31/03 EPA 8260E <br /> 1,1,1-Trichloroethane ND 5 0 " <br /> 1,1,2-Trichloroethane ND 50 <br /> Tnchloroethene ND 50 " <br /> Trichlorofluoromethane ND 50 <br /> 1,2,3-Trichloropropane ND 5 0 <br /> 1,2,4-Trimethylbenzene 150 50 " <br /> 1,3,5-Trimethylhenzene 34 50 " <br /> Vinyl acetate ND 50 " <br /> Vinyl chloride ND 10 " <br /> Xylenes(total) 360 10 <br /> Di-isopropyl ether ND 50 01/02/04li <br /> " <br /> e"'It-butyl <br /> l tert-butyl ether ND 50-amyl methyl ether ND 50 alcohol ND 50 " <br /> Surrogate 1,2-Dichlaroethane-d4 110% 66-135 12131/03 " <br /> ' Surrogate Toluene-d8 985% 72-125 <br /> Surrogate 4-Bromofluorobenzene 958% 73-125 <br /> MW-12(CML0881-11)Water Sampled 12/19/03 12 17 Received I2/23/03 10 50 <br /> Acetone ND 10 gg/L 1 CL33026 12/30/03 12/30/03 EPA 8260E <br /> Benzene 19 050 H " <br /> Bromobenzene ND 0 50 <br /> Bromochloromethane ND 0 50 <br /> ' Bromodichloromethane ND 0 50 h " X " <br /> Bromoform ND 0 50 " <br /> Bromomethane ND 10 " <br /> 2-Butanone ND 10 <br /> n-Butylbenzene ND 050 <br /> sec-Butylbenzene ND 0 50 " <br /> ter,-Butylbenzene ND 050 <br /> Carbon tetrachloride ND 050 N <br /> Chlorooenzene ND 050 <br /> Chloroethane ND 0 50 " <br /> ' Chloroform ND 050 " <br /> CA DOHS FLAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www califurnialab.com 916-638-7301 Fax 916-638-4510 <br />