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VOC ANALYTIC/ Y QC REPORT FOR�l101627 DATE PRINTED 07 FEB 1997 AQUEOUS SAMPLES ------ METHOD BLANK ------ --------------- LAB CONTROL -------------- ---------------- MATRIX QC --------- ------ LCS LCSD RPD RPD Ms MSD RPD RPO UNITS RESULT ROL FLG %REC FLG %REC FLG LCL UCL RPD UCL FLG %REC FLG %REC FLG LCL UCL RPD UCL FLG Batch VOA,8260*972015 Method 8260 - Volatile Organics, GCMS, cont - - Carbon Disulfide ug/L 0 2 - 93 37 140 17 - - - - - - Dibromochloromethane ug/L 0 0 5 - 103 - 110 - 65 142 6 30 - - - - - - - Dibromomethane ug/L 0 0 5 - 94 - 98 - 59 139 4 30 - - - - - - - - - - Dichlorodifluoromethane ug/L 0 0 5 - 79 - 87 - 30 150 9 30 - - - - - - - Ethylbenzene ug/L 0 0 5 - 114 - 122 - 80 135 7 30 - - Freon 113 ug/L 0 1 - 95 - 97 - 49 159 1 - - - - Hexachlorobutadiene ug/L 0 24 1 - 15 Q 73 - 68 140 133 36 Q - - - - - - - - - Isopropylbenzene ug/L 0 0 5 - 113 - 118 - 79 130 5 30 - - Methyl ethyl ketone ug/L 0 10 - 121 - 106 - 5 153 13 50 - - - - - - - - - hethyl isobutyl ketone ug/L 0 4 - 123 - 129 - 16 150 5 49 - - - - - - - Ilethylene chloride ug/L 0 2 - 97 - 107 - 51 139 10 30 - - - - - i4-Butylbenzene ug/L 0 15 1 - 115 - 124 - 78 134 7 30 - - - - - - - N-Propylbenzene ug/L 0 0 5 - 120 - 128 - 79 133 6 30 - - - - - - Naphthalene ug/L 0 0 5 - 94 - 106 - 51 149 13 42 - - - - Styrene ug/L 0 0 5 - 109 - 116 - 80 129 6 53 - - - - - - Trichloroethene ug/L 0 0 5 - 98 - 101 - 71 135 4 30 - - - - - Trichlorofluoromethane ug/L 0 0 5 - 99 - 96 - 58 156 4 30 - - - - - - - - - - Toluene ug/L 0 0 5 - 104 - 108 - 70 129 3 30 - - - - - - - - - - Tetrachloroethene ug/L 0 39 0 5 - 'i, - 109 - 67 145 14 30 - - - - - - - - - - Vinyl acetate ug/L 0 5 - Ii - 108 - 24 143 5 - - - Vinyl chloride ug/L 0 0 5 - - 100 - 48 140 11 30 - - - - cis-1,2-Dichloroethene ug/L 0 0 5 - jj - 104 - 54 143 5 30 - - - - - - - - - - m- and p-Xylene Isomers ug/L 0 1 - 111 - 118 - 80 136 6 30 o-Xylene ug/L 0 0 5 - 106 - 113 - 78 133 6 30 - - - - - p-Isopropyl toluene ug/L 0 0 5 - 112 - 119 - 75 136 6 30 sec-Butylbenzene ug/L 0 0 5 - 117 - 125 - 76 136 6 30 - - - - - trans-1,2-Dichloroethene ug/l. 0 0 5 - 96 - 101 - 48 134 5 30 - - - - - tert-Butylbenzene ug/L 0 0 5 - 103 - 111 - 79 129 7 30 - - - - - - - - - - [4-8romofluorobenzenel Percent 99 - - 98 - 105 - 80 111 - - - [Toluene-dB] Percent 102 - - 100 - 103 - 80 113 - - - - - - [Dibromofluoromethanel Percent 97 - - 96 - 95 - 80 114 - - - Hatch GAS*974013 Method 8015M TX - Modified 8015 � ]fi l55 - - - 101 - 111 - 70 153 9 25 - iirnzcne ug/1 0 0 5 - k13 - - - - - iuluule u - -g/1 0 0 5 - 102 - - - 72 121 - - 92 91 69 119 1 25 1thylhenzerne ug/t 0 0 5 - 91 - - - 12 115 - - 94 = 95 = 68 116 1 25 Ilethy1-tert-butylether ug/L f} 30 - 77 - - - 62 159 - - 103 89 80 176 i5 25 total Xylene lsoaiet5 ug/L 0 0 5 - 99 - - - 68 115 - - - 91 91 61 118 0 25