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Lancaster Laboratories <br /> ICSTQ J Quantitation Report GC/MS Volatiles T C S W V 5 <br /> e /chem2/HP09137 i/OSdecl6a h/wd18101 d Sample Concentration Formula On-Column Amount * (Vt/VC) <br /> ple LCSW85 LCSW65 1 3 LCS CHEV Batch W053521M Matrix WATER <br /> ect 18-DEC-2003 15 17 Analyst SAM00983 Level Low <br /> 1br0 T.me 30-MOV-2005 03 34 instrument ID UP09137 i Sample tilt /Vol 5 0000 ml (Vo) <br /> get Method W826OW m Standard Reference wdIScOl d Volume Purged 5 0 ml (Vt) <br /> nk Reference wdl8b01 d Prep Factor 1 00 <br /> List CHEV60LOW Units ug/L <br /> nternal Standards RT(+/-RT) Sean Qlon Area(+/- %Area) Conc(ext) QC Flag <br />................. ......... _... .... ...........=:.r ......=.e ....... <br /> t-Butyl Alcohol-dl0i 4 492( 0 (103) 907 65 257534( 1) 250 00 <br /> 1 Fluorobenzene 7 929( 0 003) 1978 96 933144( -2) 50 00 <br /> Chlorobenzene-d5 11 331( 0 003) 3038 117 703708( -11 50 00 <br /> 1 4-Dichlorobenmene-d4 13 192( 0 ODO) 3618 152 391713( 0) 5o 00 <br /> RETENTION TIME OUT OF RANGE . INTERNAL STANDARD OUT OF RANGE NC . NOT ABLE TO CALCULATE <br /> I S Conc OC <br /> urrogate Standards Ref RT (+/-RRT) Olon Area (on coluer) tRec flags QC Limits <br /> s `• r ' 8 •• ' i F•Oibromofluoromethane (1) 7 DOS( 000) 113242280 <br />} 45 464 91% SO - 116 <br /> 1 1 2-Oichloroethane-d4 (1) 7 461( 0 0001 102 58320 43 907 Bat 77 - 113 <br />} Toluene-d8 (2) 9 912( 0 000) 98 905459 45 363 91% s0 - 113 <br />} 4-Bromofluorobenzene 42) 12 309( 0 000) 95 359956 46 191 92t 78 - 113 <br /> RELATIVE RETENTION TIME OUT OF RANGE • = PERCENT REC OUT OF RANGE D - DILUTED OUT NC - NOT ABLE TO CALCULATE <br /> I g Cone Cone Blank Reporting <br /> arget Compounds Ref RT (+/-RRT) Olon Area (on column) (ln sample) Conc Qual Limit LOQ <br />)P Dichlorodifluoromethane c(1)•RR2`XIS('0'000) w�sa5R FS 97095 's'13^676 13 6a 2 00 5 00 <br /> 1omethane (1) 2 2534 0 000) 50 87629 14 262 14 26 1 00 5 00 <br /> i Chlcride (1) 2 391 0 0001 62 88164 15 103 15 10 1 00 5 00 <br /> Bromomethane (1) 2 734( 0 003) 94 64253 16 343 16 34 1 00 5 00 <br /> Chloroethane (1) 2 B56( 0 001) 64 51562 15 829 15 03 1 00 5 DO <br /> Trichlorofluoromethane (1) 3 164( 0 003) 101 147303 18 221 18 22 2 00 5 DO <br /> Ethanol (4) 3 35D( 0 001) 45 60485 672 650 672 65 50 00 250 00 <br /> Acrolein (1) 3 645{ 0 0001 56 185736 113 624 113 62 40 00 100 00 <br /> 1 1-Dichloroethene (1) 3 609( 0 001) 96 83048 20 $41 20 54 0 SO 5 00 <br /> Freon 113 (1) 3 B25( 0 001) 101 72264 IS 415 18 41 2 OD 10 00 <br /> Acetone (1) 3 022( 0 002) 58 215802 242 038 242 04 6 00 20 00 <br />) Carbon Disulfide (1) 4 136( 0 000) 76 253429 18 957 18 96 1 00 5 00 <br />) Methylene Chloride (1) 4 4731 0 001) 84 100820 19 525 19 52 2 00 5 OD <br />) t-Butyl Alcohol (4) 4 621(-0 001) 59 2932a4 233 698 233 70 5 00 8o 00 <br />) Acrylonitrile (1) 4 804( 0 0031 53 294143 92 096 92 10 4 00 213 00 <br />} trans-I 2-Dxchloroethene (1) 4 906( 0 001) 96 96056 20 076 20 OB 0 SD 5 00 <br />} Methyl Tertiary Butyl Ether (1) 4 91D( 0 001) 73 343539 19 933 19 93 0 50 4 00 <br />} 1 1-Dlchloroethane (1) 5 516( 0 000) 63 179232 20 373 20 37 1 OD 5 00 <br />) di-Isopropyl Ether (11 5 641( 0 000) 45 306792 19 385 19 39 0 50 4 00 <br />) Ethyl t-Butyl Ether (1) 6 167( 0 000) 59 319605 19 5e5 19 59 0 50 4 00 <br />} cia-1 2-Dzchloroethene (1) 6 350 0 000) 96 106594 20 242 20 24 0 80 5 00 <br /> 2-Butanone (1) 6 341( 0 002) 72 220668 167 887 187 89 3 00 1D 00 <br />} 2 2-Dicb1oropropane (1) 6 366( 0 000) 77 161882 21 357 21 36 1 00 5 00 <br /> Bromochloromethane (1) 6 671[ 0 001) 128 54753 19 035 19 04 1 00 5 00 <br /> CONC OUT OF CAL RANCE # . RELATIVE RETENTION TIME OUT OF RANGE <br /> Page 1 of 4 <br />