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• r <br /> nlcCamobell Analvtual, Inc. 154 w,lt,,N�,e,,;d.rm.ha,t cA 94W-1701 <br /> i,. N'rb wvv.mrcnnq+Mll a,m I:-m:nl m:nni,mru,mphdl.,m <br /> "\1"hen Oueluc( noo " Mc hone.877-252-9262 Aa'.9'5-_52-9269 <br /> NIGR Sotahwest,Inc. Client Project ID: 9773.PRI.02 Dale Sampled: 10/03/07 <br /> 315 W. Pine Street Suite S <br /> Date Received: 10/03/07 <br /> Client Contact Caryl Shechan Date Extracted: I(NO3/07 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed: 10/04/07 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> 1.Nra'I tan M,tliw MV-3S9O( Anakucal Method- 5\\'82701 \\'ork(lydcr 071111i1 <br /> IIIb Ill <br /> 0710131-003A <br /> Client ID 133 <br /> Matrix Soil <br /> Compound Concentration ` DF xq+wmnµ <br /> I n;,,,a I Compound Concentration DF <br /> Acena hthenc ND 1.0 0.33 Acena hthvlene ND 1.0 0.33 <br /> Acetochlor ND 1.0 0.33 Anthracene ND 1.0 0.33 <br /> Benzidine ND 1.0 1.6 Benzoic Acid ND LO 1.6 <br /> Benzo(a)anthracene ND 1.0 0.33 Benzothllluorambenc ND 1.0 0,33 <br /> Benzo(k luoranthene ND 1.0 0.33 13cnzo(u.h,i) ervlenc ND 1.0 0.33 <br /> Benzo(a) vrcne ND 1.0 0.33 Benzyl Alcohol ND I.0 0.66 <br /> 1.I-Bi henvl ND 1.0 033 Bis(2-chloroethox• Methane ND I.0 0.33 <br /> Bis(2-chloroethv] Ether ND 1.0 0.33 His 2-chloroisotro 1 Ether ND IA 0.33 <br /> Bis 2-cth Ihexvl)Phthalate ND 1.0 033 4-Bromrarbenyl Phenyl Ether ND 1.0 0.33 <br /> Butvlbenz•1 Phthalate ND jr) 0.33 4-Chloroaniline ND lA 0.66 <br /> 4-Chloro-3-methvl henol ND 1.0 0.33 2-Chloroma thiha bene ND 1.0 0.33 <br /> 2-Chloro heuol ND jr) 0.33 4-Chloro hcu%I Phenyl Ether ND 1.0 0.33 <br /> Chrvsene ND 1.0 0.33 Dibenzo(a,h anthracene ND 1.0 0.33 <br /> 1 Tbcnzofuran ND 1.0 0.33 Di-n-bnlVl Phthalate ND LO 0.33 <br /> 12-Dichlorobenzene ND 1.0 0.33 1,3-Dichlorobenzene ND 1.0 0.33 <br /> • 14-Dichlorobenzene ND IA 0.33 3,3-Dieblombenzidmc ND 1.0 0.66 <br /> 2.4-Dicliloro henol ND 1.0 033 Diethyl Phthnlatc ND 1.0 0.33 <br /> 2,4-Dimethv] henol ND 1.0 0.33 Dimethvl Phthalnle ND 1.0 0.33 <br /> 4.6-Dinitro-2-methvl henol ND 1.0 1.6 2,4-Dinitro henol ND 1.0 1.6 <br /> 'A-Dirraromluene ND 1.0 0.33 2,6-Dinitrotuluene ND 1.0 0.33 <br /> Di-n-octvl Phthalate ND 1.0 033 1.2-Di henvlllvdrazine ND 1.0 0.33 <br /> Pluoranthene ND 1.0 0.33 Fluorene ND 1.0 0.33 <br /> Hexachlorobenzene NI) LO 033 Hexaehlorobetadiene ND 1.0 0.33 <br /> Hexachlorocvelo entadicne ND LO 1.6 Hexaehloroethane ND 1,0 0.33 <br /> Indeno 123-ed •rene ND 1.0 0.33 Iso horone ND IA 0.33 <br /> 2-Me1h Ina hthalene ND 1.0 0,33 %Njeth I henol o-Cresol ND 1.0 0.33 <br /> 3&/or 4-1,vieth d Ihenol (M -Cres ND 1.0 0.33 Natilithalem, ND 1.0 0.33 <br /> 3-Nitroaniline ND 1.0 1.6 3-Nitroaniline ND 1.0 1.6 <br /> 4-Nitronniline NI) 1.0 L( Nitrohcnzrnc ND I.0 0.33 <br /> 2-Nitro henol NI) 1.0 1,6 4-Nm...Awn"I ND LO 1.6 <br /> N-Nitrosodi hemgamine ND 1.0 0,33 V-N'itrosoJi-n-'m tetaminc ND 1.0 0.33 <br /> Pentaehlorohcuol ND 1.0 1.6 Phrnanthrenc ND LO 033 <br /> Phenol N) 1 0 0,33 '•re c12 0 .33 <br /> 7.4-1-rich oh ' <br /> ze e ) 1.0 0,33 LT w t t o m 'of J 1.0 0.331 <br /> Surrogate Recoveries <br /> %SS 1 85 %557: 71 <br /> °%SS3: 91 %9S4: R, <br /> q. %SS6 77 <br /> Commenls: <br /> •water samples in pg/L,soil/sludge/solid samples in mgtkg,wipe samples in pglwipe,producV.0/non-aqueous liquid samples and alb WIT& <br /> SPLP extracts are reported in mg'L. <br /> ND means not detected above the reporting limit;NIA means analyte not applicable In this analysis. <br /> a)sun'ocale diluted out al range;&)low or no surrogate due to matrix interferenc, <br /> h)lighter than mater immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)sample diluted due to <br /> high organic content/matrix interference;k)reporting limit raised due to insufficient sample amount;in)reporting limit raised due to matrix <br /> interference:r)results are reponed on a dry weight basis. <br /> DHS FLAP Certification N` 1644 `-k- Angela Rydelius, Lab Manager <br />