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110 2nd Avenue S- '137,Pacheco,CA 94553-5560 <br /> McCampbell Ana cal, Inc. Telephone:92hs{1620 Fax:925-798-1622 <br /> Website:www.mccampbell.com E-mail:main@mccampbell.com <br /> ! Cambria Env.Technology Client Project ID: #424-1840700,1;Jimco Date Sampled: 05/26/04 <br /> Truck Plaza Date Received: 05/27/04 <br /> 5900 Hollis St,Suite A <br /> Client Contact: Matt Meyers Date Extracted: 05/27/04 <br /> Emeryville,CA 94608 Client P.O.: Date Analyzed: 05/28/04 <br /> Volatiles Organics by P&T and GUMS(Basic Target List)' <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order: 0405449 <br /> Lab ID 0405449-OOIA <br /> _ Client ID SP-IA-D <br /> Matrix Soil <br /> Rc rtin� <br /> Rep-tin� <br /> Compound Concentration* DF m;t Compound i Concentration* DF ; Limit <br /> Acetone ND 1.0 i 50 �_Acrolein(Propenal) ` ND 1.0 50 <br /> Acrylonitrile _ _ _ _ - ND 11- I- 20 tert-Am I methyl ether(TAME) _�_ ND - _1 1.0 5.0 <br /> Benzene _ ND y 1.0 5.0 Bromobenzene ND _ 1.0 5.0_ <br /> Bromochloromethane ND 1.0 1 5.0 Bromodichloromethane ND _1.0 5.0 <br /> ---�---'-T-� <br /> _Bromoform- _ - ND 1.0 5.0 Bromomethane ND 1.0 1 5.0 <br /> 2-Butanone(MEK) ND 1.0 10 t-But 1 alcohol(TBA) ND 1.0 25 <br /> n-Butyl benzene ND 1.0 5.0 see-Butyl benzene ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Carbon Disulfide ND 1.0 5.0 <br /> Carbon Tetrachloride_ ND 1.0 5.0 Chlorobenzene ND 1.0 5.0 <br /> Chloroethane _ _ND 1.0 5.0 2-Chloroeth 1 Vinyl Ether ND _ 1.0 10 <br /> Chloroform a - _ ND LO 5.0 Chloromethane ND 1.0 5.0 <br /> _- - -- -- <br /> 2-Chlorotoluene ND 1.0 5.0 4-Chlorotoluene ND 1.0 5.0 <br /> ---- ---- ----- - -1 --_ -.-r .- - - -- --- - - - <br /> Dibromochloromethane ND _ 1.0 5.0 1,2-Dtbromo-3-chloropropane ND 1.0 5.0_ <br /> _ ND_ 1.0 5.0 Dibromomethane ND 1.0 5.0 <br /> I,_-Dibromoethane(EDB) _ _ - ----�------- -- <br /> ---- <br /> l,2-Dichlorobenzene _ND i LO 5.0 1,3-Dichlorobenzene ND 1.0 1 5.0 <br /> l,4-Dichlorobenzene________ V__N�LO 5.0 Dichlorodifluoromethane ND 1.0 _5.0 <br /> 1,1-Dichlor_oethane _ ND 1 1.0 5.0 1,2-Dichloroethane(1,2-DCA) ND 1.0 5.0 <br /> 1,1-_Dichloroethene _ _ ND 1.0 5.0 cis-1,2-Dichloroethene ND 1.0 5.0 <br /> trans-l,2-D_ichloroethene 1 ND 1.0 5.0 1,2-Dichloropropane ND_ 1.0 5.0 <br /> 1.3-Dichloropropane ND LO_ 50 2,2-Dichloropropane ND _ LO 5.0 <br /> 1,1-Dichloro�ropene _ -ND l.0 5 0 cis-1,3-Dichloropropene _ ND rt 1.0T 5.0 <br /> trans-13-Dichloropro�ene ND LO 5.0 Diiso ro 1 ether(DIPE) - ND - - 1.0 - 5.0 <br /> -- --- ---- - - -- _ -�- <br /> Ethyibenzene _ND LO_ 5.0 Ethyl tert-butyl ether(ETBE) ND _ LO 5.0 <br /> -- t <br /> Hexachlorobutadiene ND LO -5.0 I Hexachloroethane ND 1.0 5.0 <br /> 2-Hexanone _ _ _ ND 1.0_ 5.0 Iso ro (benzene ND 1.0 5.0 <br /> 4-Isopropyl toluene ND 1.0 5.0 Meth I-t-but 1 ether(MTBE) ND 1.0 X5.0 <br /> Methene chloride_- -i ND L0 5.0 4-Meth 1-2- entanone(MIRK) ND 1.0 5.0_ <br /> Naphthalene - ND l.0 5.0 Nitrobenzene ND 1.0 100 <br /> n-Prrop I benzene ND 1.0 5.0 f Styrene ND _ LO_ 5.0 <br /> 1,1,1,2-Tetrachloroethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> Tetrachloroethene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> 1,2,3-T_richlorobenzene ND 1.0 5.0 1,2,4-Trichlorobenzene ND 1.0 5.0 <br /> 1,1,1-Trichloroethane _ ND 1.0 5.0 j 1,1,2-Trichloroethane ND 1.0 5.0 <br /> Trichloroethene _ ND i 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> 1,2,3-Trichloropropane ND 1.0 5.01,1,2-Trichloro-1,2,2-trifluoroethane ND 1.0 100 <br /> 1,2,4-Trimethylbenzene ND 1 1.0 5.0 1,3,5-Trimeth lbenzene ND j 1.0 5.0 <br /> Vin I Chloride ND 1.0 5.0 1 X lenes ND 1.0 5.0 <br /> Surrogate Recoveries(%) <br /> %SS 1: -- 98.6 %SS2: 103 -- <br /> %nSS3: --- --- - 10? <br /> Comments: <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in IA.- .,soiUsludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oiUnon-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> DHS Certification No. 1644 �°^ Angela Rydelius,Lab Manager <br />