Laserfiche WebLink
I 10 2nd Asenue South PD7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925 798 1622 <br /> Website www mccampbell coni E marl mai c(�imccarnpb0l corn <br /> QC SUMMARY REPORT FOR SW8260B <br /> W O Sample Matrix Water QC Matnx Water WorkOrder 0509017 <br /> EPA Method SW8260B Extraction SW5030B BatchlD 17820 Spiked Sample ID 0509024-002C <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria (%) <br /> pg1L pg1L %Rec % Rec % RPD %Rec %Rec % RPD MS 1 MSD LCS 1 LCSD <br /> tent-Amyl methyl ether(TAME) ND 10 93 5 933 0 194 923 91 5 0 865 70- 130 70- 130 <br /> t-Butyl alcohol(TBA) ND 50 104 996 3 89 98 1 912 736 70- 130 70- 130 <br /> 1,2-Dibromoethane(EDB) ND 10 966 994 280 966 942 2 53 70- 130 70- 130 <br /> 1 2-Dichloroethane(1,2-DCA) ND 10 110 111 0 921 115 110 433 70-130 70- 130 <br /> Dnsopropyl ether(DIPE) ND 10 117 117 0 118 118 0 70- 130 70- 130 <br /> Ethanol ND 500 114 116 1 38 115 114 1 26 70- 130 70- 130 <br /> Ethyl tert butyl ether(ETBE) ND 10 964 985 208 984 973 1 16 j 70- 130 70- 130 <br /> Methanol ND 2500 967 102 5 80 106 105 0 602 70-130 70- 130 <br /> Methyl-t-butyl ether(MTBE) ND 10 973 975 0 266 100 954 472 70-130 70- 130 <br /> %SSI 100 10 103 101 2 07 104 102 1 61 70- 130 70- 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> • <br /> BATCH 17820 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0509017-005C 8131/05 9 25 AM 9102/05 9102105 5 54 PM <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100`(MS-Sample)/(Amount Spiked) RPD=100'(MS- MSD)/((MS+MSD)12) <br /> MS 1 MSD spike recoveries and 1 or%RPD may fall outside of laboratory acceptance entena due to one or more of the following reasons a)the sample is inhomogenous AND <br /> contains significant concentrations of analyle relative to the amount spiked or b)the spiked sample's matrix interferes with the spike recovery <br /> NIA=not enough sample to perform matrix spoke and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for sod matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> Wrtory extraction solvents such as methylene chloride and acetone may occasionally appear in the method blank at low levels <br /> DHS Certification No 1644 QA/QC Officer <br />